Quantitation Report (QT Reviewed) Data Path : Z:\VOASRV\HPCHEM1\MSVOA_U\DATA\VU061318\ Data File : VU024508.D Acq On : 13 Jun 2018 15:27 Operator : MD/SY Sample : PB110190TB Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 11 Sample Multiplier: 1 Quant Time: Jun 13 17:14:09 2018 Quant Method : Z:\VOASRV\HPCHEM1\MSVOA_U\METHOD\82U061318W.M Quant Title : SW846 8260 QLast Update : Wed Jun 13 13:55:26 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 4.99 168 207597 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 5.89 114 349381 50.00 ug/l 0.00 63) Chlorobenzene-d5 9.09 117 327361 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 11.49 152 187344 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 5.32 65 163232 48.16 ug/l 0.00 Spiked Amount 50.000 Recovery = 96.32% 35) Dibromofluoromethane 4.89 113 141840 48.92 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.84% 50) Toluene-d8 7.57 98 510071 48.23 ug/l 0.00 Spiked Amount 50.000 Recovery = 96.46% 62) 4-Bromofluorobenzene 10.31 95 199091 47.41 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.82% Target Compounds Qvalue 16) Acetone 2.32 43 19597 10.762 ug/l 99 18) Methyl Acetate 2.62 43 15986 4.095 ug/l 93 20) Methylene Chloride 2.71 84 3404 1.191 ug/l # 93 76) 1,2,3-Trichloropropane 10.31 75 100145 24.280 ug/l # 36 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed