Quantitation Report (QT/LSC Reviewed) Data Path : Z:\VOASRV\HPCHEM1\MSVOA_U\DATA\VU061318\ Data File : VU024512.D Acq On : 13 Jun 2018 16:59 Operator : MD/SY Sample : PB110190ZHE#11 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 15 Sample Multiplier: 1 Quant Time: Jun 14 02:27:41 2018 Quant Method : Z:\VOASRV\HPCHEM1\MSVOA_U\METHOD\82U061318W.M Quant Title : SW846 8260 QLast Update : Wed Jun 13 13:55:26 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 4.99 168 179468 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 5.89 114 303217 50.00 ug/l 0.00 63) Chlorobenzene-d5 9.09 117 287872 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 11.49 152 166333 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 5.32 65 139655 47.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.34% 35) Dibromofluoromethane 4.89 113 120805 48.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 96.02% 50) Toluene-d8 7.57 98 439588 47.89 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.78% 62) 4-Bromofluorobenzene 10.31 95 172408 47.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.62% Target Compounds Qvalue 16) Acetone 2.33 43 19454 12.358 ug/l 98 18) Methyl Acetate 2.62 43 16715 4.953 ug/l 96 20) Methylene Chloride 2.71 84 3710 1.502 ug/l 93 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed