Quantitation Report (QT Reviewed) Data Path : Z:\VOASRV\HPCHEM1\MSVOA_U\DATA\VU061318\ Data File : VU024513.D Acq On : 13 Jun 2018 17:22 Operator : MD/SY Sample : PB110190ZHE#12 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 16 Sample Multiplier: 1 Quant Time: Jun 14 02:31:14 2018 Quant Method : Z:\VOASRV\HPCHEM1\MSVOA_U\METHOD\82U061318W.M Quant Title : SW846 8260 QLast Update : Wed Jun 13 13:55:26 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 4.99 168 184474 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 5.89 114 313564 50.00 ug/l 0.00 63) Chlorobenzene-d5 9.09 117 305550 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 11.49 152 175112 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 5.32 65 146780 48.74 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.48% 35) Dibromofluoromethane 4.89 113 127038 48.82 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.64% 50) Toluene-d8 7.57 98 462886 48.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.52% 62) 4-Bromofluorobenzene 10.31 95 184274 48.89 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.78% Target Compounds Qvalue 16) Acetone 2.32 43 17253 10.662 ug/l 99 18) Methyl Acetate 2.62 43 16663 4.804 ug/l 98 20) Methylene Chloride 2.71 84 3663 1.443 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed