Quantitation Report (QT Reviewed) Data Path : Z:\VOASRV\HPCHEM1\MSVOA_U\DATA\VU061318\ Data File : VU024514.D Acq On : 13 Jun 2018 17:45 Operator : MD/SY Sample : PB110190ZHE#13 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 17 Sample Multiplier: 1 Quant Time: Jun 14 02:36:11 2018 Quant Method : Z:\VOASRV\HPCHEM1\MSVOA_U\METHOD\82U061318W.M Quant Title : SW846 8260 QLast Update : Wed Jun 13 13:55:26 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 4.99 168 187126 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 5.89 114 317683 50.00 ug/l 0.00 63) Chlorobenzene-d5 9.09 117 308228 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 11.49 152 178984 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 5.32 65 146234 47.87 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.74% 35) Dibromofluoromethane 4.89 113 129317 49.05 ug/l 0.00 Spiked Amount 50.000 Recovery = 98.10% 50) Toluene-d8 7.57 98 470120 48.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.76% 62) 4-Bromofluorobenzene 10.31 95 185195 48.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.00% Target Compounds Qvalue 16) Acetone 2.32 43 18798 11.453 ug/l 96 18) Methyl Acetate 2.62 43 17255 4.904 ug/l 100 20) Methylene Chloride 2.71 84 3950 1.534 ug/l # 89 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed