Quantitation Report (QT Reviewed) Data Path : Z:\VOASRV\HPCHEM1\MSVOA_U\DATA\VU061318\ Data File : VU024517.D Acq On : 13 Jun 2018 18:55 Operator : MD/SY Sample : PB110190ZHE#16 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 20 Sample Multiplier: 1 Quant Time: Jun 14 02:47:28 2018 Quant Method : Z:\VOASRV\HPCHEM1\MSVOA_U\METHOD\82U061318W.M Quant Title : SW846 8260 QLast Update : Wed Jun 13 13:55:26 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 4.99 168 185778 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 5.89 114 314413 50.00 ug/l 0.00 63) Chlorobenzene-d5 9.09 117 303862 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 11.49 152 175777 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 5.32 65 145495 47.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.94% 35) Dibromofluoromethane 4.89 113 125603 48.14 ug/l 0.00 Spiked Amount 50.000 Recovery = 96.28% 50) Toluene-d8 7.57 98 464927 48.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.70% 62) 4-Bromofluorobenzene 10.31 95 183472 48.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.10% Target Compounds Qvalue 16) Acetone 2.32 43 17802 10.924 ug/l 98 18) Methyl Acetate 2.62 43 17744 5.079 ug/l 100 20) Methylene Chloride 2.71 84 3364 1.316 ug/l 87 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed