Quantitation Report (QT Reviewed) Data Path : Z:\VOASRV\HPCHEM1\MSVOA_U\DATA\VU061318\ Data File : VU024522.D Acq On : 13 Jun 2018 20:50 Operator : MD/SY Sample : J3461-08 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 25 Sample Multiplier: 1 Quant Time: Jun 14 02:56:31 2018 Quant Method : Z:\VOASRV\HPCHEM1\MSVOA_U\METHOD\82U061318W.M Quant Title : SW846 8260 QLast Update : Wed Jun 13 13:55:26 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 4.99 168 184298 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 5.89 114 315337 50.00 ug/l 0.00 63) Chlorobenzene-d5 9.09 117 300969 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 11.49 152 177102 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 5.32 65 142457 47.35 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.70% 35) Dibromofluoromethane 4.89 113 128065 48.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.86% 50) Toluene-d8 7.57 98 461470 48.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 96.68% 62) 4-Bromofluorobenzene 10.31 95 183101 48.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 96.62% Target Compounds Qvalue 16) Acetone 2.32 43 22170 13.714 ug/l 97 18) Methyl Acetate 2.62 43 15499 4.472 ug/l 94 20) Methylene Chloride 2.71 84 4120 1.624 ug/l 93 51) 4-Methyl-2-Pentanone 7.47 43 2474 0.564 ug/l 92 65) Chlorobenzene 9.12 112 2090 0.272 ug/l # 85 76) 1,2,3-Trichloropropane 10.31 75 90958 23.328 ug/l # 36 81) trans-1,4-Dichloro-2-buten 10.31 75 90958 53.990 ug/l # 100 95) Naphthalene 13.76 128 1155 0.767 ug/l # 78 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed