Quantitation Report (QT Reviewed) Data Path : Z:\VOASRV\HPCHEM1\MSVOA_U\DATA\VU061318\ Data File : VU024523.D Acq On : 13 Jun 2018 21:14 Operator : MD/SY Sample : J3461-07 Misc : 5.0mL/MSVOA_U/WATER ALS Vial : 26 Sample Multiplier: 1 Quant Time: Jun 14 03:39:22 2018 Quant Method : Z:\VOASRV\HPCHEM1\MSVOA_U\METHOD\82U061318W.M Quant Title : SW846 8260 QLast Update : Wed Jun 13 13:55:26 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 4.99 168 180919 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 5.89 114 309533 50.00 ug/l 0.00 63) Chlorobenzene-d5 9.09 117 299710 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 11.49 152 175851 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 5.32 65 138987 47.06 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.12% 35) Dibromofluoromethane 4.89 113 125883 49.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 98.00% 50) Toluene-d8 7.57 98 455692 48.63 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.26% 62) 4-Bromofluorobenzene 10.31 95 180144 48.42 ug/l 0.00 Spiked Amount 50.000 Recovery = 96.84% Target Compounds Qvalue 16) Acetone 2.33 43 16740 10.549 ug/l 98 18) Methyl Acetate 2.62 43 16590 4.876 ug/l 97 20) Methylene Chloride 2.71 84 3391 1.362 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed