Quantitation Report    (QT/LSC Reviewed)

  Data Path : W:\HPCHEM1\MSVOA_V\DATA\VV052618\
  Data File : VV006068.D                                          
  Acq On    : 26 May 2018  20:37
  Operator  : SY/MD
  Sample    : J3090-19 100X
  Misc      : 5.0 mL/MSVOA_V/WATER
  ALS Vial  : 22   Sample Multiplier: 1

  Quant Time: May 28 04:07:44 2018
  Quant Method : W:\HPCHEM1\MSVOA_V\METHOD\SOMVLM052518WMA.M
  Quant Title  : VOC Analysis
  QLast Update : Mon May 28 02:03:29 2018
  Response via : Initial Calibration

   Internal Standards                R.T. QIon  Response  Conc Units Dev(Min)
   --------------------------------------------------------------------------
     1) 1,4-Difluorobenzene          5.67  114   171496    50.00 ug/L    0.00
    28) Chlorobenzene-d5             8.90  117   156006    50.00 ug/L    0.00
    60) 1,4-Dichlorobenzene-d4      11.30  152    60810    50.00 ug/L    0.00

   System Monitoring Compounds                                        
     4) Vinyl Chloride-d3            1.32   65    54729    45.69 ug/L    0.00  
     Spiked Amount     50.000   Range  60 - 135    Recovery   =   91.38% 
     7) Chloroethane-d5              1.55   69    12504    14.76 ug/L   -0.02  
     Spiked Amount     50.000   Range  70 - 130    Recovery   =   29.52%#
    11) 1,1-Dichloroethene-d2        2.12   63    77752    34.88 ug/L   -0.01  
     Spiked Amount     50.000   Range  60 - 125    Recovery   =   69.76% 
    21) 2-Butanone-d5                3.95   46    55532    80.95 ug/L    0.00  
     Spiked Amount    100.000   Range  40 - 130    Recovery   =   80.95% 
    24) Chloroform-d                 4.41   84   104041    46.08 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 125    Recovery   =   92.16% 
    26) 1,2-Dichloroethane-d4        5.09   65    70778    48.02 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 125    Recovery   =   96.04% 
    32) Benzene-d6                   5.10   84   206529    49.80 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 125    Recovery   =   99.60% 
    36) 1,2-Dichloropropane-d6       6.12   67    65895    50.03 ug/L    0.00  
     Spiked Amount     50.000   Range  70 - 120    Recovery   =  100.06% 
    41) Toluene-d8                   7.37   98   178307    46.47 ug/L    0.00  
     Spiked Amount     50.000   Range  80 - 120    Recovery   =   92.94% 
    43) trans-1,3-Dichloropropene-   7.67   79    26644    43.93 ug/L    0.00  
     Spiked Amount     50.000   Range  60 - 125    Recovery   =   87.86% 
    47) 2-Hexanone-d5                8.14   63    51775   100.02 ug/L    0.00  
     Spiked Amount    100.000   Range  45 - 130    Recovery   =  100.02% 
    57) 1,1,2,2-Tetrachloroethane-  10.27   84    90422    49.93 ug/L    0.00  
     Spiked Amount     50.000   Range  65 - 120    Recovery   =   99.86% 
    64) 1,2-Dichlorobenzene-d4      11.68  152    65576    54.22 ug/L    0.00  
     Spiked Amount     50.000   Range  80 - 120    Recovery   =  108.44% 

   Target Compounds                                                   Qvalue
    34) Trichloroethene              5.96   95    28976    23.03 ug/L      98
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   (#) = qualifier out of range (m) = manual integration (+) = signals summed