Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052218\ Data File : VW002795.D Acq On : 22 May 2018 19:49 Operator : JC/SY Sample : VSTDCCC025 Misc : 5.00G/10ML/MSVOA_W/SOIL ALS Vial : 1 Sample Multiplier: 1 Quant Time: May 23 05:41:33 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\SOM2WLM052218S.M Quant Title : VOC Analysis QLast Update : Tue May 22 12:32:39 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 8.85 114 305592 25.00 ug/L 0.00 28) Chlorobenzene-d5 11.64 117 290140 25.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 13.57 152 155937 25.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 2.34 65 91584 23.36 ug/L 0.00 Spiked Amount 25.000 Range 30 - 150 Recovery = 93.44% 7) Chloroethane-d5 2.89 69 84443 24.09 ug/L 0.00 Spiked Amount 25.000 Range 30 - 150 Recovery = 96.36% 10) 1,1-Dichloroethene-d2 4.01 63 163766 23.85 ug/L 0.00 Spiked Amount 25.000 Range 45 - 110 Recovery = 95.40% 20) 2-Butanone-d5 7.08 46 72453 45.32 ug/L 0.00 Spiked Amount 50.000 Range 20 - 135 Recovery = 90.64% 24) Chloroform-d 7.65 84 184756 25.22 ug/L 0.00 Spiked Amount 25.000 Range 40 - 150 Recovery = 100.88% 26) 1,2-Dichloroethane-d4 8.31 65 110887 25.07 ug/L 0.00 Spiked Amount 25.000 Range 70 - 130 Recovery = 100.28% 29) Benzene-d6 8.27 84 342459 24.82 ug/L 0.00 Spiked Amount 25.000 Range 20 - 135 Recovery = 99.28% 33) 1,2-Dichloropropane-d6 9.28 67 112329 25.19 ug/L 0.00 Spiked Amount 25.000 Range 70 - 120 Recovery = 100.76% 37) Toluene-d8 10.33 98 341003 25.04 ug/L 0.00 Spiked Amount 25.000 Range 30 - 130 Recovery = 100.16% 38) trans-1,3-Dichloropropene- 10.59 79 53752 25.20 ug/L 0.00 Spiked Amount 25.000 Range 30 - 135 Recovery = 100.80% 39) 2-Hexanone-d5 10.93 63 62051 49.04 ug/L 0.00 Spiked Amount 50.000 Range 20 - 135 Recovery = 98.08% 48) 1,1,2,2-Tetrachloroethane- 12.70 84 121810 24.92 ug/L 0.00 Spiked Amount 25.000 Range 45 - 120 Recovery = 99.68% 61) 1,2-Dichlorobenzene-d4 13.87 152 141695 24.72 ug/L 0.00 Spiked Amount 25.000 Range 75 - 120 Recovery = 98.88% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 50002 27.42 ug/L 97 3) Chloromethane 2.21 50 78922 25.02 ug/L 98 5) Vinyl chloride 2.36 62 130007 24.24 ug/L 97 6) Bromomethane 2.77 94 89656 24.41 ug/L 100 8) Chloroethane 2.92 64 81587 23.90 ug/L 97 9) Trichlorofluoromethane 3.25 101 48047 20.70 ug/L 97 11) 1,1,2-Trichloro-1,2,2-trif 4.05 101 90973 24.48 ug/L # 71 12) 1,1-Dichloroethene 4.03 96 86666 23.65 ug/L 92 13) Acetone 4.12 43 52102 36.84 ug/L 99 14) Carbon disulfide 4.37 76 267940 23.73 ug/L 98 15) Methyl Acetate 4.67 43 55484 21.55 ug/L 100 16) Methylene chloride 4.90 84 93058 23.56 ug/L 97 17) Methyl tert-butyl Ether 5.43 73 162204 24.00 ug/L # 90 18) trans-1,2-Dichloroethene 5.41 96 90608 23.62 ug/L 95 19) 1,1-Dichloroethane 6.21 63 161872 24.06 ug/L 99 21) 2-Butanone 7.18 43 76110 40.66 ug/L 98 22) cis-1,2-Dichloroethene 7.17 96 99994 23.81 ug/L 94 23) Bromochloromethane 7.51 128 49003 23.95 ug/L 97 25) Chloroform 7.68 83 174008 23.92 ug/L 100 27) 1,2-Dichloroethane 8.40 62 128102 24.17 ug/L 96 30) Cyclohexane 7.95 56 145366 23.68 ug/L 99 31) 1,1,1-Trichloroethane 7.87 97 130674 23.28 ug/L 98 32) Carbon tetrachloride 8.07 117 133384 23.72 ug/L 99 34) Benzene 8.32 78 376958 23.95 ug/L 100 35) Trichloroethene 9.10 95 99380 23.10 ug/L 99 36) Methylcyclohexane 9.34 83 170357 23.97 ug/L 100 40) 1,2-Dichloropropane 9.37 63 99646 24.42 ug/L 100 41) Bromodichloromethane 9.65 83 129393 24.32 ug/L 100 42) cis-1,3-Dichloropropene 10.08 75 151640 24.15 ug/L 100 43) 4-Methyl-2-pentanone 10.22 43 167122 45.49 ug/L 99 44) Toluene 10.40 91 412643 24.04 ug/L 100 45) trans-1,3-Dichloropropene 10.61 75 138254 24.16 ug/L 97 46) 1,1,2-Trichloroethane 10.79 97 80376 23.78 ug/L 96 47) Tetrachloroethene 10.87 164 86608 23.27 ug/L 97 49) 2-Hexanone 10.98 43 122810 45.29 ug/L 97 50) Dibromochloromethane 11.13 129 98070 24.03 ug/L 97 51) 1,2-Dibromoethane 11.24 107 82046 23.89 ug/L 100 52) Chlorobenzene 11.66 112 271642 23.88 ug/L 98 53) Ethylbenzene 11.74 91 461489 23.93 ug/L 98 54) m,p-Xylene 11.85 106 176291 24.01 ug/L 98 55) o-xylene 12.18 106 169966 24.36 ug/L 98 56) Styrene 12.19 104 302723 24.77 ug/L 98 57) Isopropylbenzene 12.48 105 457816 24.04 ug/L 100 58) 1,1,2,2-Tetrachloroethane 12.73 83 112206 23.56 ug/L 99 59) 1,2,3-Trichloropropane 12.78 75 82800 23.11 ug/L 98 62) Bromoform 12.36 173 64579 23.61 ug/L 99 63) 1,3-Dichlorobenzene 13.51 146 220066 23.68 ug/L 99 64) 1,4-Dichlorobenzene 13.59 146 230942 23.70 ug/L 97 65) 1,2-Dichlorobenzene 13.88 146 220143 24.38 ug/L 96 66) 1,2-Dibromo-3-chloropropan 14.50 75 19837 22.34 ug/L 98 67) 1,3,5-Trichlorobenzene 14.64 180 178965 23.92 ug/L 99 68) 1,2,4-trichlorobenzene 15.15 180 151886 24.15 ug/L 99 69) Naphthalene 15.38 128 313515 24.63 ug/L 100 70) 1,2,3-Trichlorobenzene 15.57 180 147092 24.90 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed