Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052218\ Data File : VW002814.D Acq On : 23 May 2018 04:57 Operator : JC/SY Sample : VSTDCCC025EC Misc : 5.00G/10ML/MSVOA_W/SOIL ALS Vial : 1 Sample Multiplier: 1 Quant Time: May 23 06:58:57 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\SOM2WLM052218S.M Quant Title : VOC Analysis QLast Update : Wed May 23 06:53:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 8.85 114 308803 25.00 ug/L 0.00 28) Chlorobenzene-d5 11.64 117 297948 25.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 13.57 152 155263 25.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 2.34 65 84530 21.34 ug/L 0.00 Spiked Amount 25.000 Range 30 - 150 Recovery = 85.36% 7) Chloroethane-d5 2.89 69 76136 21.49 ug/L 0.00 Spiked Amount 25.000 Range 30 - 150 Recovery = 85.96% 10) 1,1-Dichloroethene-d2 4.01 63 151201 21.79 ug/L 0.00 Spiked Amount 25.000 Range 45 - 110 Recovery = 87.16% 20) 2-Butanone-d5 7.08 46 78740 48.74 ug/L 0.00 Spiked Amount 50.000 Range 20 - 135 Recovery = 97.48% 24) Chloroform-d 7.65 84 177743 24.01 ug/L 0.00 Spiked Amount 25.000 Range 40 - 150 Recovery = 96.04% 26) 1,2-Dichloroethane-d4 8.31 65 108607 24.30 ug/L 0.00 Spiked Amount 25.000 Range 70 - 130 Recovery = 97.20% 29) Benzene-d6 8.27 84 329012 23.22 ug/L 0.00 Spiked Amount 25.000 Range 20 - 135 Recovery = 92.88% 33) 1,2-Dichloropropane-d6 9.28 67 107679 23.51 ug/L 0.00 Spiked Amount 25.000 Range 70 - 120 Recovery = 94.04% 37) Toluene-d8 10.33 98 321850 23.02 ug/L 0.00 Spiked Amount 25.000 Range 30 - 130 Recovery = 92.08% 38) trans-1,3-Dichloropropene- 10.59 79 47500 21.69 ug/L 0.00 Spiked Amount 25.000 Range 30 - 135 Recovery = 86.76% 39) 2-Hexanone-d5 10.93 63 64945 49.98 ug/L 0.00 Spiked Amount 50.000 Range 20 - 135 Recovery = 99.96% 48) 1,1,2,2-Tetrachloroethane- 12.70 84 120258 23.96 ug/L 0.00 Spiked Amount 25.000 Range 45 - 120 Recovery = 95.84% 61) 1,2-Dichlorobenzene-d4 13.87 152 136148 23.86 ug/L 0.00 Spiked Amount 25.000 Range 75 - 120 Recovery = 95.44% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 45417m 24.65 ug/L 3) Chloromethane 2.21 50 76947 24.14 ug/L 98 5) Vinyl chloride 2.36 62 121048 22.33 ug/L 99 6) Bromomethane 2.78 94 83401 22.47 ug/L 100 8) Chloroethane 2.92 64 76590 22.20 ug/L 94 9) Trichlorofluoromethane 3.25 101 46269 19.72 ug/L 99 11) 1,1,2-Trichloro-1,2,2-trif 4.04 101 86132 22.93 ug/L # 68 12) 1,1-Dichloroethene 4.03 96 83057 22.43 ug/L 97 13) Acetone 4.12 43 51764 36.22 ug/L 99 14) Carbon disulfide 4.37 76 258448 22.66 ug/L 99 15) Methyl Acetate 4.67 43 60419 23.22 ug/L 99 16) Methylene chloride 4.91 84 91881 23.02 ug/L 98 17) Methyl tert-butyl Ether 5.42 73 168515 24.68 ug/L 99 18) trans-1,2-Dichloroethene 5.41 96 86976 22.44 ug/L 96 19) 1,1-Dichloroethane 6.21 63 160956 23.67 ug/L 99 21) 2-Butanone 7.18 43 80938 42.79 ug/L 98 22) cis-1,2-Dichloroethene 7.17 96 98691 23.26 ug/L 98 23) Bromochloromethane 7.51 128 49290 23.84 ug/L 96 25) Chloroform 7.68 83 172813 23.51 ug/L 99 27) 1,2-Dichloroethane 8.40 62 129667 24.21 ug/L 99 30) Cyclohexane 7.95 56 138856 22.03 ug/L 99 31) 1,1,1-Trichloroethane 7.87 97 128247 22.25 ug/L 99 32) Carbon tetrachloride 8.07 117 126213 21.86 ug/L 99 34) Benzene 8.32 78 372208 23.02 ug/L 100 35) Trichloroethene 9.09 95 100268 22.69 ug/L 98 36) Methylcyclohexane 9.34 83 161730 22.16 ug/L 99 40) 1,2-Dichloropropane 9.37 63 95248 22.73 ug/L 99 41) Bromodichloromethane 9.65 83 127254 23.29 ug/L 98 42) cis-1,3-Dichloropropene 10.08 75 139748 21.68 ug/L 100 43) 4-Methyl-2-pentanone 10.22 43 177032 46.93 ug/L 99 44) Toluene 10.40 91 408323 23.17 ug/L 98 45) trans-1,3-Dichloropropene 10.61 75 127539 21.70 ug/L 99 46) 1,1,2-Trichloroethane 10.79 97 81576 23.50 ug/L 95 47) Tetrachloroethene 10.87 164 83286 21.79 ug/L 97 49) 2-Hexanone 10.98 43 129012 46.33 ug/L 98 50) Dibromochloromethane 11.13 129 97662 23.30 ug/L 97 51) 1,2-Dibromoethane 11.24 107 82972 23.52 ug/L 97 52) Chlorobenzene 11.66 112 268095 22.95 ug/L 99 53) Ethylbenzene 11.74 91 451449 22.80 ug/L 99 54) m,p-Xylene 11.85 106 171131 22.70 ug/L 99 55) o-xylene 12.18 106 164840 23.01 ug/L 94 56) Styrene 12.19 104 295044 23.51 ug/L 94 57) Isopropylbenzene 12.48 105 439197 22.46 ug/L 100 58) 1,1,2,2-Tetrachloroethane 12.73 83 113414 23.19 ug/L 98 59) 1,2,3-Trichloropropane 12.78 75 86414 23.48 ug/L 100 62) Bromoform 12.36 173 64333 23.63 ug/L 99 63) 1,3-Dichlorobenzene 13.51 146 209174 22.60 ug/L 98 64) 1,4-Dichlorobenzene 13.59 146 219875 22.66 ug/L 98 65) 1,2-Dichlorobenzene 13.88 146 211468 23.52 ug/L 97 66) 1,2-Dibromo-3-chloropropan 14.50 75 20820 23.55 ug/L 90 67) 1,3,5-Trichlorobenzene 14.64 180 161522 21.68 ug/L 100 68) 1,2,4-trichlorobenzene 15.15 180 141325 22.56 ug/L 99 69) Naphthalene 15.38 128 316390 24.96 ug/L 100 70) 1,2,3-Trichlorobenzene 15.57 180 139471 23.72 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed