Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052418\ Data File : VW002837.D Acq On : 24 May 2018 10:20 Operator : JC/SY Sample : VSTDCCC025 Misc : 5.00G/10ML/MSVOA_W/SOIL ALS Vial : 1 Sample Multiplier: 1 Quant Time: May 25 07:52:09 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\SOM2WLM052218S.M Quant Title : VOC Analysis QLast Update : Thu May 24 18:38:29 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 8.84 114 333570 25.00 ug/L 0.00 28) Chlorobenzene-d5 11.64 117 318610 25.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 13.57 152 166722 25.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 2.34 65 79903 18.67 ug/L 0.00 Spiked Amount 25.000 Range 30 - 150 Recovery = 74.68% 7) Chloroethane-d5 2.89 69 74501 19.47 ug/L 0.00 Spiked Amount 25.000 Range 30 - 150 Recovery = 77.88% 10) 1,1-Dichloroethene-d2 4.01 63 156961 20.94 ug/L 0.00 Spiked Amount 25.000 Range 45 - 110 Recovery = 83.76% 20) 2-Butanone-d5 7.08 46 61705 35.36 ug/L 0.00 Spiked Amount 50.000 Range 20 - 135 Recovery = 70.72% 24) Chloroform-d 7.65 84 175189 21.91 ug/L 0.00 Spiked Amount 25.000 Range 40 - 150 Recovery = 87.64% 26) 1,2-Dichloroethane-d4 8.31 65 101936 21.11 ug/L 0.00 Spiked Amount 25.000 Range 70 - 130 Recovery = 84.44% 29) Benzene-d6 8.27 84 318273 21.01 ug/L 0.00 Spiked Amount 25.000 Range 20 - 135 Recovery = 84.04% 33) 1,2-Dichloropropane-d6 9.28 67 104571 21.36 ug/L 0.00 Spiked Amount 25.000 Range 70 - 120 Recovery = 85.44% 37) Toluene-d8 10.33 98 315478 21.10 ug/L 0.00 Spiked Amount 25.000 Range 30 - 130 Recovery = 84.40% 38) trans-1,3-Dichloropropene- 10.59 79 49549 21.16 ug/L 0.00 Spiked Amount 25.000 Range 30 - 135 Recovery = 84.64% 39) 2-Hexanone-d5 10.93 63 49470 35.60 ug/L 0.00 Spiked Amount 50.000 Range 20 - 135 Recovery = 71.20% 48) 1,1,2,2-Tetrachloroethane- 12.70 84 106220 19.79 ug/L 0.00 Spiked Amount 25.000 Range 45 - 120 Recovery = 79.16% 61) 1,2-Dichlorobenzene-d4 13.87 152 132031 21.55 ug/L 0.00 Spiked Amount 25.000 Range 75 - 120 Recovery = 86.20% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 60470 30.38 ug/L 90 3) Chloromethane 2.21 50 82589 23.99 ug/L 97 5) Vinyl chloride 2.36 62 132249 22.59 ug/L 100 6) Bromomethane 2.78 94 89942 22.43 ug/L 99 8) Chloroethane 2.92 64 82473 22.13 ug/L 98 9) Trichlorofluoromethane 3.25 101 56739 22.39 ug/L 99 11) 1,1,2-Trichloro-1,2,2-trif 4.04 101 94280 23.24 ug/L # 67 12) 1,1-Dichloroethene 4.03 96 90628 22.66 ug/L 92 13) Acetone 4.12 43 55811 36.15 ug/L 99 14) Carbon disulfide 4.37 76 280546 22.77 ug/L 99 15) Methyl Acetate 4.67 43 51892 18.46 ug/L 99 16) Methylene chloride 4.91 84 94933 22.02 ug/L 94 17) Methyl tert-butyl Ether 5.42 73 157549 21.36 ug/L 98 18) trans-1,2-Dichloroethene 5.41 96 95163 22.73 ug/L 98 19) 1,1-Dichloroethane 6.21 63 171248 23.31 ug/L 97 21) 2-Butanone 7.17 43 73228 35.84 ug/L 98 22) cis-1,2-Dichloroethene 7.17 96 103531 22.59 ug/L 96 23) Bromochloromethane 7.51 128 49909 22.35 ug/L 98 25) Chloroform 7.67 83 182031 22.93 ug/L 99 27) 1,2-Dichloroethane 8.40 62 128108 22.15 ug/L 98 30) Cyclohexane 7.95 56 153556 22.78 ug/L 99 31) 1,1,1-Trichloroethane 7.87 97 140017 22.71 ug/L 98 32) Carbon tetrachloride 8.07 117 140560 22.76 ug/L 98 34) Benzene 8.32 78 394620 22.83 ug/L 100 35) Trichloroethene 9.09 95 104841 22.19 ug/L 99 36) Methylcyclohexane 9.34 83 182280 23.35 ug/L 99 40) 1,2-Dichloropropane 9.37 63 102911 22.97 ug/L 99 41) Bromodichloromethane 9.65 83 133951 22.92 ug/L 96 42) cis-1,3-Dichloropropene 10.08 75 156975 22.77 ug/L 98 43) 4-Methyl-2-pentanone 10.22 43 148708 36.86 ug/L 99 44) Toluene 10.39 91 432739 22.96 ug/L 99 45) trans-1,3-Dichloropropene 10.61 75 143243 22.79 ug/L 99 46) 1,1,2-Trichloroethane 10.79 97 79362 21.38 ug/L 98 47) Tetrachloroethene 10.87 164 92079 22.53 ug/L 99 49) 2-Hexanone 10.98 43 112142 37.66 ug/L 97 50) Dibromochloromethane 11.13 129 98792 22.05 ug/L 97 51) 1,2-Dibromoethane 11.24 107 79001 20.95 ug/L 95 52) Chlorobenzene 11.66 112 286581 22.94 ug/L 99 53) Ethylbenzene 11.74 91 487693 23.03 ug/L 99 54) m,p-Xylene 11.85 106 187030 23.20 ug/L 98 55) o-xylene 12.18 106 179218 23.39 ug/L 99 56) Styrene 12.19 104 313558 23.36 ug/L 95 57) Isopropylbenzene 12.48 105 485387 23.21 ug/L 100 58) 1,1,2,2-Tetrachloroethane 12.73 83 103252 19.74 ug/L 99 59) 1,2,3-Trichloropropane 12.78 75 76455 19.43 ug/L 99 62) Bromoform 12.35 173 61829 21.15 ug/L 99 63) 1,3-Dichlorobenzene 13.51 146 231239 23.27 ug/L 99 64) 1,4-Dichlorobenzene 13.59 146 241502 23.18 ug/L 98 65) 1,2-Dichlorobenzene 13.88 146 221919 22.99 ug/L 98 66) 1,2-Dibromo-3-chloropropan 14.49 75 17387 18.32 ug/L 97 67) 1,3,5-Trichlorobenzene 14.64 180 186321 23.29 ug/L 99 68) 1,2,4-trichlorobenzene 15.15 180 154894 23.03 ug/L 98 69) Naphthalene 15.38 128 288227 21.18 ug/L 99 70) 1,2,3-Trichlorobenzene 15.57 180 147191 23.31 ug/L 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed