Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052418\ Data File : VW002855.D Acq On : 24 May 2018 18:51 Operator : JC/SY Sample : VSTDCC025EC Misc : 5.00G/10ML/MSVOA_W/SOIL ALS Vial : 1 Sample Multiplier: 1 Quant Time: May 25 07:58:49 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\SOM2WLM052218S.M Quant Title : VOC Analysis QLast Update : Fri May 25 07:55:38 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) 1,4-Difluorobenzene 8.85 114 292431 25.00 ug/L 0.00 28) Chlorobenzene-d5 11.64 117 281885 25.00 ug/L 0.00 60) 1,4-Dichlorobenzene-d4 13.57 152 149917 25.00 ug/L 0.00 System Monitoring Compounds 4) Vinyl Chloride-d3 2.34 65 77327 20.62 ug/L 0.00 Spiked Amount 25.000 Range 30 - 150 Recovery = 82.48% 7) Chloroethane-d5 2.89 69 69633 20.76 ug/L 0.00 Spiked Amount 25.000 Range 30 - 150 Recovery = 83.04% 10) 1,1-Dichloroethene-d2 4.01 63 135057 20.56 ug/L 0.00 Spiked Amount 25.000 Range 45 - 110 Recovery = 82.24% 20) 2-Butanone-d5 7.09 46 79212 51.78 ug/L 0.00 Spiked Amount 50.000 Range 20 - 135 Recovery = 103.56% 24) Chloroform-d 7.65 84 163609 23.34 ug/L 0.00 Spiked Amount 25.000 Range 40 - 150 Recovery = 93.36% 26) 1,2-Dichloroethane-d4 8.31 65 98722 23.32 ug/L 0.00 Spiked Amount 25.000 Range 70 - 130 Recovery = 93.28% 29) Benzene-d6 8.27 84 289665 21.61 ug/L 0.00 Spiked Amount 25.000 Range 20 - 135 Recovery = 86.44% 33) 1,2-Dichloropropane-d6 9.28 67 95321 22.00 ug/L 0.00 Spiked Amount 25.000 Range 70 - 120 Recovery = 88.00% 37) Toluene-d8 10.33 98 283966 21.46 ug/L 0.00 Spiked Amount 25.000 Range 30 - 130 Recovery = 85.84% 38) trans-1,3-Dichloropropene- 10.59 79 44676 21.56 ug/L 0.00 Spiked Amount 25.000 Range 30 - 135 Recovery = 86.24% 39) 2-Hexanone-d5 10.93 63 66386 54.00 ug/L 0.00 Spiked Amount 50.000 Range 20 - 135 Recovery = 108.00% 48) 1,1,2,2-Tetrachloroethane- 12.70 84 119067 25.07 ug/L 0.00 Spiked Amount 25.000 Range 45 - 120 Recovery = 100.28% 61) 1,2-Dichlorobenzene-d4 13.87 152 123318 22.38 ug/L 0.00 Spiked Amount 25.000 Range 75 - 120 Recovery = 89.52% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 64512 36.97 ug/L 97 3) Chloromethane 2.21 50 85458 28.31 ug/L 99 5) Vinyl chloride 2.36 62 131942 25.70 ug/L 95 6) Bromomethane 2.77 94 85696 24.38 ug/L 100 8) Chloroethane 2.92 64 77268 23.65 ug/L 98 9) Trichlorofluoromethane 3.24 101 38251 17.22 ug/L 99 11) 1,1,2-Trichloro-1,2,2-trif 4.04 101 83884 23.59 ug/L # 50 12) 1,1-Dichloroethene 4.02 96 81553 23.26 ug/L 99 13) Acetone 4.12 43 56526 41.77 ug/L 99 14) Carbon disulfide 4.37 76 246719 22.84 ug/L 99 15) Methyl Acetate 4.67 43 63820 25.90 ug/L 99 16) Methylene chloride 4.91 84 87262 23.09 ug/L 98 17) Methyl tert-butyl Ether 5.43 73 152374 23.56 ug/L 99 18) trans-1,2-Dichloroethene 5.41 96 85468 23.28 ug/L 98 19) 1,1-Dichloroethane 6.21 63 155368 24.13 ug/L 98 21) 2-Butanone 7.18 43 91621 51.15 ug/L 97 22) cis-1,2-Dichloroethene 7.17 96 96486 24.01 ug/L 97 23) Bromochloromethane 7.51 128 47025 24.02 ug/L 98 25) Chloroform 7.67 83 168789 24.25 ug/L 99 27) 1,2-Dichloroethane 8.40 62 126266 24.90 ug/L 99 30) Cyclohexane 7.95 56 140517 23.56 ug/L 98 31) 1,1,1-Trichloroethane 7.87 97 123390 22.62 ug/L 98 32) Carbon tetrachloride 8.07 117 126025 23.07 ug/L 98 34) Benzene 8.32 78 363660 23.78 ug/L 100 35) Trichloroethene 9.09 95 96699 23.13 ug/L 98 36) Methylcyclohexane 9.34 83 162168 23.48 ug/L 98 40) 1,2-Dichloropropane 9.37 63 95239 24.02 ug/L 100 41) Bromodichloromethane 9.65 83 125447 24.27 ug/L 99 42) cis-1,3-Dichloropropene 10.08 75 142103 23.30 ug/L 99 43) 4-Methyl-2-pentanone 10.22 43 186540 52.27 ug/L 98 44) Toluene 10.39 91 398365 23.89 ug/L 98 45) trans-1,3-Dichloropropene 10.61 75 132146 23.77 ug/L 99 46) 1,1,2-Trichloroethane 10.79 97 80442 24.49 ug/L 97 47) Tetrachloroethene 10.87 164 83976 23.22 ug/L 99 49) 2-Hexanone 10.98 43 140263 53.24 ug/L 97 50) Dibromochloromethane 11.13 129 96199 24.26 ug/L 97 51) 1,2-Dibromoethane 11.24 107 80697 24.18 ug/L 100 52) Chlorobenzene 11.66 112 261086 23.62 ug/L 99 53) Ethylbenzene 11.74 91 445813 23.79 ug/L 100 54) m,p-Xylene 11.85 106 171074 23.98 ug/L 98 55) o-xylene 12.18 106 161020 23.76 ug/L 97 56) Styrene 12.19 104 287817 24.24 ug/L 100 57) Isopropylbenzene 12.48 105 441650 23.87 ug/L 100 58) 1,1,2,2-Tetrachloroethane 12.73 83 114378 24.72 ug/L 98 59) 1,2,3-Trichloropropane 12.78 75 88449 25.41 ug/L 100 62) Bromoform 12.35 173 64879 24.68 ug/L 99 63) 1,3-Dichlorobenzene 13.51 146 209024 23.39 ug/L 98 64) 1,4-Dichlorobenzene 13.59 146 221140 23.61 ug/L 97 65) 1,2-Dichlorobenzene 13.88 146 207563 23.91 ug/L 99 66) 1,2-Dibromo-3-chloropropan 14.49 75 21707 25.43 ug/L 96 67) 1,3,5-Trichlorobenzene 14.64 180 168907 23.48 ug/L 98 68) 1,2,4-trichlorobenzene 15.15 180 141097 23.33 ug/L 97 69) Naphthalene 15.38 128 321843 26.30 ug/L 99 70) 1,2,3-Trichlorobenzene 15.57 180 140225 24.69 ug/L 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed