Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_W\Data\VW052518\ Data File : VW002857.D Acq On : 24 May 2018 21:56 Operator : JC/SY Sample : VSTDCCC050 Misc : 5.00G/10ML/MSVOA_W/SOIL ALS Vial : 27 Sample Multiplier: 1 Quant Time: May 25 01:34:13 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\82W051518S.M Quant Title : SW846 8260 QLast Update : Tue May 15 03:32:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 7.95 168 188178 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 8.85 114 292102 50.00 ug/l 0.00 63) Chlorobenzene-d5 11.64 117 277906 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 13.57 152 157858 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 8.31 65 117262 60.30 ug/l 0.00 Spiked Amount 50.000 Recovery = 120.60% 35) Dibromofluoromethane 7.88 113 101609 54.83 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.66% 50) Toluene-d8 10.33 98 378892 53.74 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.48% 62) 4-Bromofluorobenzene 12.63 95 142650 55.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 110.66% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 49111 67.63 ug/l 100 3) Chloromethane 2.21 50 84129 60.57 ug/l 94 4) Vinyl Chloride 2.36 62 130067 59.71 ug/l 99 5) Bromomethane 2.76 94 97575 54.64 ug/l 95 6) Chloroethane 2.92 64 83761 55.88 ug/l 99 7) Trichlorofluoromethane 3.24 101 36819 38.36 ug/l 98 8) Diethyl Ether 3.67 74 78900 68.70 ug/l 98 9) 1,1,2-Trichlorotrifluoroet 4.04 101 88360 55.57 ug/l 98 10) Methyl Iodide 4.26 142 135065 53.30 ug/l 100 11) Tert butyl alcohol 5.20 59 45322 303.20 ug/l 98 12) 1,1-Dichloroethene 4.02 96 84981 53.99 ug/l 98 13) Acrolein 3.88 56 67308 457.07 ug/l 98 14) Allyl chloride 4.65 41 109777 47.00 ug/l 99 15) Acrylonitrile 5.37 53 135010 325.98 ug/l 99 16) Acetone 4.12 43 120904 294.51 ug/l 99 17) Carbon Disulfide 4.37 76 213365 49.27 ug/l 99 18) Methyl Acetate 4.67 43 88873 74.26 ug/l 99 19) Methyl tert-butyl Ether 5.43 73 183910 63.59 ug/l 96 20) Methylene Chloride 4.91 84 98113 60.66 ug/l 97 21) trans-1,2-Dichloroethene 5.41 96 93144 54.74 ug/l 95 22) Diisopropyl ether 6.31 45 309511 59.82 ug/l 98 23) Vinyl Acetate 6.26 43 1001410 319.37 ug/l 100 24) 1,1-Dichloroethane 6.21 63 181398 58.17 ug/l 99 25) 2-Butanone 7.18 43 200485 345.35 ug/l 98 26) 2,2-Dichloropropane 7.17 77 79575 45.54 ug/l 99 27) cis-1,2-Dichloroethene 7.17 96 110902 57.13 ug/l 99 28) Bromochloromethane 7.51 49 83876 60.26 ug/l 98 29) Tetrahydrofuran 7.53 42 131380 362.28 ug/l 98 30) Chloroform 7.67 83 199861 60.03 ug/l 94 31) Cyclohexane 7.95 56 134029 48.52 ug/l 98 32) 1,1,1-Trichloroethane 7.87 97 135663 54.02 ug/l 99 36) 1,1-Dichloropropene 8.08 75 136132 52.81 ug/l 99 37) Ethyl Acetate 7.26 43 87148 68.17 ug/l 99 38) Carbon Tetrachloride 8.07 117 134457 53.27 ug/l 95 39) Methylcyclohexane 9.34 83 148670 50.35 ug/l 98 40) Benzene 8.32 78 411720 55.63 ug/l 100 41) Methacrylonitrile 7.49 41 51663 72.20 ug/l 92 42) 1,2-Dichloroethane 8.40 62 144336 61.41 ug/l 99 43) Isopropyl Acetate 8.43 43 165776 67.42 ug/l 98 44) Trichloroethene 9.09 130 110319 54.39 ug/l 99 45) 1,2-Dichloropropane 9.37 63 111271 59.00 ug/l 99 46) Dibromomethane 9.46 93 65879 61.39 ug/l 99 47) Bromodichloromethane 9.65 83 151023 60.34 ug/l 100 48) Methyl methacrylate 9.44 41 85145 71.47 ug/l 94 49) 1,4-Dioxane 9.45 88 23910 1336.91 ug/l 97 51) 4-Methyl-2-Pentanone 10.22 43 472780 350.20 ug/l 100 52) Toluene 10.39 92 265171 56.67 ug/l 99 53) t-1,3-Dichloropropene 10.61 75 151844 60.00 ug/l 99 54) cis-1,3-Dichloropropene 10.08 75 165993 58.84 ug/l 99 55) 1,1,2-Trichloroethane 10.79 97 93637 61.93 ug/l 98 56) Ethyl methacrylate 10.65 69 123451 67.00 ug/l 99 57) 1,3-Dichloropropane 10.94 76 157567 62.83 ug/l 100 58) 2-Chloroethyl Vinyl ether 9.93 63 292613 323.51 ug/l 99 59) 2-Hexanone 10.98 43 336977 361.55 ug/l 100 60) Dibromochloromethane 11.13 129 112261 62.93 ug/l 100 61) 1,2-Dibromoethane 11.24 107 92329 63.27 ug/l 99 64) Tetrachloroethene 10.87 164 117496 59.98 ug/l 97 65) Chlorobenzene 11.66 112 305136 55.13 ug/l 99 66) 1,1,1,2-Tetrachloroethane 11.74 131 114506 57.79 ug/l 99 67) Ethyl Benzene 11.74 91 521166 55.40 ug/l 99 68) m/p-Xylenes 11.85 106 405027 110.74 ug/l 100 69) o-Xylene 12.18 106 193742 55.75 ug/l 100 70) Styrene 12.19 104 335086 57.94 ug/l 100 71) Bromoform 12.35 173 74406 63.91 ug/l 99 73) Isopropylbenzene 12.48 105 522793 53.73 ug/l 100 74) N-amyl acetate 12.28 43 163809 66.08 ug/l 100 75) 1,1,2,2-Tetrachloroethane 12.73 83 122557 62.16 ug/l 99 76) 1,2,3-Trichloropropane 12.77 75 89044m 59.67 ug/l 77) Bromobenzene 12.76 156 139001 55.99 ug/l 99 78) n-propylbenzene 12.81 91 639588 54.42 ug/l 99 79) 2-Chlorotoluene 12.90 91 370796 55.56 ug/l 99 80) 1,3,5-Trimethylbenzene 12.95 105 454737 54.76 ug/l 100 81) trans-1,4-Dichloro-2-buten 12.52 75 33670 61.52 ug/l 98 82) 4-Chlorotoluene 13.00 91 396665 54.97 ug/l 100 83) tert-Butylbenzene 13.21 119 396611 55.31 ug/l 99 84) 1,2,4-Trimethylbenzene 13.26 105 477294 55.37 ug/l 99 85) sec-Butylbenzene 13.40 105 557749 54.13 ug/l 100 86) p-Isopropyltoluene 13.51 119 504079 54.39 ug/l 100 87) 1,3-Dichlorobenzene 13.51 146 275310 54.82 ug/l 99 88) 1,4-Dichlorobenzene 13.59 146 273776 54.80 ug/l 100 89) n-Butylbenzene 13.83 91 473155 53.97 ug/l 100 90) Hexachloroethane 14.10 117 91990 55.43 ug/l 99 91) 1,2-Dichlorobenzene 13.88 146 258380 56.71 ug/l 99 92) 1,2-Dibromo-3-Chloropropan 14.50 75 22540 64.80 ug/l 98 93) 1,2,4-Trichlorobenzene 15.15 180 184704 55.68 ug/l 99 94) Hexachlorobutadiene 15.25 225 98370 53.30 ug/l 99 95) Naphthalene 15.38 128 387698 64.28 ug/l 99 96) 1,2,3-Trichlorobenzene 15.57 180 172551 58.14 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed 82W051518S.M Fri May 25 01:36:01 2018