Quantitation Report (Not Reviewed) Data Path : W:\HPCHEM1\MSVOA_W\Data\VW052518\ Data File : VW0028BL.D Acq On : 24 May 2018 22:22 Operator : JC/SY Sample : VW0525SBL01 Misc : 5.00G/10ML/MSVOA_W/SOIL ALS Vial : 28 Sample Multiplier: 1 Quant Time: May 25 01:44:54 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\82W051518S.M Quant Title : SW846 8260 QLast Update : Tue May 15 03:32:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 7.95 168 180552 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 8.85 114 290405 50.00 ug/l 0.00 63) Chlorobenzene-d5 11.64 117 272354 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 13.57 152 140720 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 8.31 65 118111 63.30 ug/l 0.00 Spiked Amount 50.000 Recovery = 126.60% 35) Dibromofluoromethane 7.88 113 102605 55.69 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.38% 50) Toluene-d8 10.33 98 361026 51.51 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.02% 62) 4-Bromofluorobenzene 12.63 95 126733 49.45 ug/l 0.00 Spiked Amount 50.000 Recovery = 98.90% Target Compounds Qvalue 8) Diethyl Ether 3.67 74 2314 2.100 ug/l 92 11) Tert butyl alcohol 5.19 59 575 4.009 ug/l 95 16) Acetone 4.12 43 9335 23.699 ug/l 91 20) Methylene Chloride 4.91 84 2658 Below Cal # 84 25) 2-Butanone 7.18 43 1450 2.603 ug/l # 80 29) Tetrahydrofuran 7.53 42 490 1.408 ug/l # 64 31) Cyclohexane 7.95 56 4554 1.718 ug/l # 8 36) 1,1-Dichloropropene 7.95 75 13550 5.287 ug/l # 48 38) Carbon Tetrachloride 7.95 117 16925 6.745 ug/l # 19 49) 1,4-Dioxane 9.67 88 19 1.069 ug/l # 1 76) 1,2,3-Trichloropropane 12.63 75 66623 50.086 ug/l # 100 81) trans-1,4-Dichloro-2-buten 12.63 75 66623 136.558 ug/l # 8 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed 82W051518S.M Fri May 25 08:00:46 2018