Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052518\ Quantitation Report (QT Reviewed) Data File : VW002857.D Acq On : 24 May 2018 21:29 Operator : JC/SY Sample : VSTDCCC050 Misc : 5.00G/5ML/MSVOA_W/SOIL ALS Vial : 26 Sample Multiplier: 1 Quant Time: May 25 08:55:39 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\82W051518S.M Quant Title : SW846 8260 QLast Update : Tue May 15 03:32:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 7.95 168 188259 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 8.85 114 286321 50.00 ug/l 0.00 63) Chlorobenzene-d5 11.64 117 274358 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 13.57 152 152123 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 8.31 65 115072 59.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 118.30% 35) Dibromofluoromethane 7.88 113 102442 56.40 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.80% 50) Toluene-d8 10.33 98 382938 55.41 ug/l 0.00 Spiked Amount 50.000 Recovery = 110.82% 62) 4-Bromofluorobenzene 12.63 95 142788 56.51 ug/l 0.00 Spiked Amount 50.000 Recovery = 113.02% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 45340 62.41 ug/l 92 3) Chloromethane 2.21 50 77602 55.85 ug/l 99 4) Vinyl Chloride 2.36 62 118430 54.35 ug/l 96 5) Bromomethane 2.76 94 92530 51.79 ug/l 98 6) Chloroethane 2.92 64 78778 52.53 ug/l 96 7) Trichlorofluoromethane 3.23 101 34060 35.47 ug/l 96 8) Diethyl Ether 3.67 74 70873 61.68 ug/l 98 9) 1,1,2-Trichlorotrifluoroet 4.04 101 90432 56.85 ug/l 97 10) Methyl Iodide 4.26 142 126398 49.86 ug/l 97 11) Tert butyl alcohol 5.20 59 40914 273.59 ug/l 98 12) 1,1-Dichloroethene 4.02 96 84009 53.35 ug/l 98 13) Acrolein 3.89 56 66002 448.01 ug/l 99 14) Allyl chloride 4.65 41 102442 43.84 ug/l 99 15) Acrylonitrile 5.37 53 123943 299.13 ug/l 98 16) Acetone 4.12 43 105843 257.71 ug/l 99 17) Carbon Disulfide 4.37 76 213727 49.33 ug/l 98 18) Methyl Acetate 4.67 43 81054 67.70 ug/l 100 19) Methyl tert-butyl Ether 5.43 73 171708 59.35 ug/l 97 20) Methylene Chloride 4.90 84 94209 58.10 ug/l 95 21) trans-1,2-Dichloroethene 5.40 96 92546 54.37 ug/l 99 22) Diisopropyl ether 6.32 45 298835 57.73 ug/l 98 23) Vinyl Acetate 6.26 43 943675 300.83 ug/l 100 24) 1,1-Dichloroethane 6.21 63 177863 57.02 ug/l 100 25) 2-Butanone 7.18 43 186267 320.72 ug/l 100 26) 2,2-Dichloropropane 7.16 77 78128 44.70 ug/l 97 27) cis-1,2-Dichloroethene 7.17 96 107898 55.56 ug/l 98 28) Bromochloromethane 7.51 49 82988 59.60 ug/l 97 29) Tetrahydrofuran 7.54 42 120096 331.02 ug/l 99 30) Chloroform 7.68 83 193284 58.03 ug/l 94 31) Cyclohexane 7.95 56 134173 48.55 ug/l 96 32) 1,1,1-Trichloroethane 7.87 97 134919 53.70 ug/l 100 36) 1,1-Dichloropropene 8.08 75 137255 54.32 ug/l 99 37) Ethyl Acetate 7.26 43 79680 63.59 ug/l 100 38) Carbon Tetrachloride 8.07 117 135566 54.80 ug/l 94 39) Methylcyclohexane 9.34 83 152864 52.82 ug/l 99 40) Benzene 8.32 78 406665 56.06 ug/l 99 41) Methacrylonitrile 7.48 41 46122 65.76 ug/l 94 42) 1,2-Dichloroethane 8.40 62 137952 59.88 ug/l 99 43) Isopropyl Acetate 8.43 43 150553 62.46 ug/l 99 44) Trichloroethene 9.09 130 110360 55.51 ug/l 100 45) 1,2-Dichloropropane 9.37 63 106547 57.64 ug/l 100 46) Dibromomethane 9.46 93 63197 60.08 ug/l 99 47) Bromodichloromethane 9.65 83 147620 60.17 ug/l 100 48) Methyl methacrylate 9.45 41 78798 67.48 ug/l 94 49) 1,4-Dioxane 9.46 88 21945 1251.81 ug/l 98 51) 4-Methyl-2-Pentanone 10.22 43 435789 329.31 ug/l 99 52) Toluene 10.39 92 260476 56.79 ug/l 99 53) t-1,3-Dichloropropene 10.61 75 143168 57.72 ug/l 95 54) cis-1,3-Dichloropropene 10.08 75 160569 58.06 ug/l 99 55) 1,1,2-Trichloroethane 10.79 97 89883 60.65 ug/l 98 56) Ethyl methacrylate 10.65 69 113158 62.66 ug/l 99 57) 1,3-Dichloropropane 10.94 76 149792 60.94 ug/l 100 58) 2-Chloroethyl Vinyl ether 9.93 63 276959 312.38 ug/l 100 59) 2-Hexanone 10.98 43 308261 337.42 ug/l 99 60) Dibromochloromethane 11.13 129 106827 61.09 ug/l 99 61) 1,2-Dibromoethane 11.24 107 87298 61.03 ug/l 100 64) Tetrachloroethene 10.87 164 112741 58.30 ug/l 96 65) Chlorobenzene 11.66 112 299197 54.75 ug/l 100 66) 1,1,1,2-Tetrachloroethane 11.74 131 110618 56.55 ug/l 99 67) Ethyl Benzene 11.74 91 512970 55.24 ug/l 99 68) m/p-Xylenes 11.85 106 397395 110.06 ug/l 100 69) o-Xylene 12.18 106 188700 55.00 ug/l 99 70) Styrene 12.19 104 323722 56.69 ug/l 100 71) Bromoform 12.35 173 70576 61.41 ug/l # 100 73) Isopropylbenzene 12.48 105 518014 55.24 ug/l 99 74) N-amyl acetate 12.28 43 147916 61.92 ug/l 98 75) 1,1,2,2-Tetrachloroethane 12.73 83 114379 60.20 ug/l 98 76) 1,2,3-Trichloropropane 12.77 75 85172m 59.23 ug/l 77) Bromobenzene 12.76 156 134776 56.33 ug/l 100 78) n-propylbenzene 12.81 91 629984 55.63 ug/l 99 79) 2-Chlorotoluene 12.90 91 360951 56.13 ug/l 99 80) 1,3,5-Trimethylbenzene 12.95 105 445797 55.71 ug/l 100 81) trans-1,4-Dichloro-2-buten 12.52 75 31758 60.22 ug/l 98 82) 4-Chlorotoluene 13.00 91 385749 55.47 ug/l 100 83) tert-Butylbenzene 13.22 119 388958 56.28 ug/l 99 84) 1,2,4-Trimethylbenzene 13.26 105 464894 55.96 ug/l 98 85) sec-Butylbenzene 13.40 105 548924 55.28 ug/l 99 86) p-Isopropyltoluene 13.51 119 493356 55.24 ug/l 100 87) 1,3-Dichlorobenzene 13.51 146 268039 55.39 ug/l 99 88) 1,4-Dichlorobenzene 13.59 146 266922 55.44 ug/l 99 89) n-Butylbenzene 13.83 91 467274 55.31 ug/l 99 90) Hexachloroethane 14.10 117 91725 57.35 ug/l 97 91) 1,2-Dichlorobenzene 13.88 146 249198 56.76 ug/l 99 92) 1,2-Dibromo-3-Chloropropan 14.49 75 20343 60.69 ug/l 98 93) 1,2,4-Trichlorobenzene 15.15 180 176614 55.25 ug/l 99 94) Hexachlorobutadiene 15.25 225 97906 55.05 ug/l 99 95) Naphthalene 15.38 128 360825 62.08 ug/l 99 96) 1,2,3-Trichlorobenzene 15.57 180 163833 57.28 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed