Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052518\ Quantitation Report (QT Reviewed) Data File : VW002860.D Acq On : 24 May 2018 23:15 Operator : JC/SY Sample : VW0525SBS01 Misc : 5.00G/5ML/MSVOA_W/SOIL ALS Vial : 30 Sample Multiplier: 1 Quant Time: May 25 08:59:46 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\82W051518S.M Quant Title : SW846 8260 QLast Update : Tue May 15 03:32:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 7.95 168 183000 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 8.85 114 284841 50.00 ug/l 0.00 63) Chlorobenzene-d5 11.64 117 267526 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 13.57 152 147000 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 8.31 65 111228 58.82 ug/l 0.00 Spiked Amount 50.000 Recovery = 117.64% 35) Dibromofluoromethane 7.88 113 98630 54.58 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.16% 50) Toluene-d8 10.33 98 369641 53.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.54% 62) 4-Bromofluorobenzene 12.63 95 132967 52.89 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.78% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 15508 21.96 ug/l 94 3) Chloromethane 2.21 50 29323 21.71 ug/l 99 4) Vinyl Chloride 2.35 62 45554 21.51 ug/l 93 5) Bromomethane 2.76 94 36937 21.27 ug/l 91 6) Chloroethane 2.92 64 30179 20.70 ug/l 90 7) Trichlorofluoromethane 3.23 101 13404 14.36 ug/l 89 8) Diethyl Ether 3.67 74 28227 25.27 ug/l 100 9) 1,1,2-Trichlorotrifluoroet 4.04 101 33218 21.48 ug/l 97 10) Methyl Iodide 4.26 142 52301 21.22 ug/l 99 11) Tert butyl alcohol 5.20 59 16555 113.89 ug/l # 90 12) 1,1-Dichloroethene 4.03 96 33453 21.86 ug/l 96 13) Acrolein 3.89 56 10873 75.93 ug/l 99 14) Allyl chloride 4.65 41 41124 18.11 ug/l 98 15) Acrylonitrile 5.37 53 47618 118.23 ug/l 97 16) Acetone 4.12 43 41794 104.69 ug/l 98 17) Carbon Disulfide 4.37 76 88230 20.95 ug/l 99 18) Methyl Acetate 4.67 43 27355 23.50 ug/l 98 19) Methyl tert-butyl Ether 5.42 73 63529 22.59 ug/l 99 20) Methylene Chloride 4.92 84 39981 23.73 ug/l 94 21) trans-1,2-Dichloroethene 5.40 96 36344 21.97 ug/l 95 22) Diisopropyl ether 6.31 45 112938 22.45 ug/l 96 23) Vinyl Acetate 6.26 43 341030 111.84 ug/l 99 24) 1,1-Dichloroethane 6.20 63 70161 23.14 ug/l 98 25) 2-Butanone 7.18 43 67733 119.98 ug/l 95 26) 2,2-Dichloropropane 7.16 77 29873 17.58 ug/l 100 27) cis-1,2-Dichloroethene 7.17 96 40670 21.54 ug/l 98 28) Bromochloromethane 7.51 49 32746 24.19 ug/l 98 29) Tetrahydrofuran 7.54 42 43296 122.77 ug/l 98 30) Chloroform 7.68 83 75392 23.28 ug/l 97 31) Cyclohexane 7.95 56 53990 20.10 ug/l 97 32) 1,1,1-Trichloroethane 7.87 97 52375 21.45 ug/l 100 36) 1,1-Dichloropropene 8.08 75 53409 21.25 ug/l 100 37) Ethyl Acetate 7.26 43 29263 23.47 ug/l 98 38) Carbon Tetrachloride 8.07 117 50954 20.70 ug/l 97 39) Methylcyclohexane 9.34 83 55991 19.45 ug/l 93 40) Benzene 8.32 78 159219 22.06 ug/l 95 41) Methacrylonitrile 7.49 41 17378 24.91 ug/l 93 42) 1,2-Dichloroethane 8.40 62 54716 23.87 ug/l 98 43) Isopropyl Acetate 8.43 43 54448 22.71 ug/l 99 44) Trichloroethene 9.09 130 43124 21.80 ug/l 90 45) 1,2-Dichloropropane 9.37 63 41083 22.34 ug/l 99 46) Dibromomethane 9.46 93 24530 23.44 ug/l 97 47) Bromodichloromethane 9.65 83 54572 22.36 ug/l 97 48) Methyl methacrylate 9.44 41 28002 24.10 ug/l 93 49) 1,4-Dioxane 9.46 88 7987 457.97 ug/l 98 51) 4-Methyl-2-Pentanone 10.22 43 153804 116.83 ug/l 99 52) Toluene 10.40 92 100168 21.95 ug/l 99 53) t-1,3-Dichloropropene 10.61 75 49897 20.22 ug/l 96 54) cis-1,3-Dichloropropene 10.08 75 58265 21.18 ug/l 99 55) 1,1,2-Trichloroethane 10.79 97 33115 22.46 ug/l 96 56) Ethyl methacrylate 10.65 69 39476 21.97 ug/l 98 57) 1,3-Dichloropropane 10.94 76 56804 23.23 ug/l 98 58) 2-Chloroethyl Vinyl ether 9.93 63 100906 114.40 ug/l 98 59) 2-Hexanone 10.98 43 107180 117.93 ug/l 97 60) Dibromochloromethane 11.13 129 38674 22.23 ug/l 99 61) 1,2-Dibromoethane 11.24 107 32103 22.56 ug/l 98 64) Tetrachloroethene 10.87 164 45269 24.01 ug/l 98 65) Chlorobenzene 11.66 112 114192 21.43 ug/l 99 66) 1,1,1,2-Tetrachloroethane 11.74 131 41091 21.54 ug/l 100 67) Ethyl Benzene 11.74 91 191016 21.09 ug/l 99 68) m/p-Xylenes 11.85 106 147045 41.76 ug/l 100 69) o-Xylene 12.18 106 68181 20.38 ug/l 98 70) Styrene 12.19 104 120381 21.62 ug/l 98 71) Bromoform 12.36 173 24733 22.07 ug/l # 96 73) Isopropylbenzene 12.48 105 186666 20.60 ug/l 100 74) N-amyl acetate 12.28 43 52462 22.73 ug/l 98 75) 1,1,2,2-Tetrachloroethane 12.73 83 41565 22.64 ug/l 99 76) 1,2,3-Trichloropropane 12.78 75 32094m 23.10 ug/l 77) Bromobenzene 12.76 156 50055 21.65 ug/l 99 78) n-propylbenzene 12.82 91 229852 21.00 ug/l 99 79) 2-Chlorotoluene 12.90 91 131349 21.14 ug/l 100 80) 1,3,5-Trimethylbenzene 12.96 105 163902 21.20 ug/l 98 81) trans-1,4-Dichloro-2-buten 12.52 75 10312 20.23 ug/l 97 82) 4-Chlorotoluene 13.00 91 142873 21.26 ug/l 99 83) tert-Butylbenzene 13.22 119 137620 20.61 ug/l 100 84) 1,2,4-Trimethylbenzene 13.26 105 170423 21.23 ug/l 98 85) sec-Butylbenzene 13.40 105 200139 20.86 ug/l 99 86) p-Isopropyltoluene 13.51 119 177441 20.56 ug/l 99 87) 1,3-Dichlorobenzene 13.51 146 98388 21.04 ug/l 99 88) 1,4-Dichlorobenzene 13.58 146 101293 21.77 ug/l 100 89) n-Butylbenzene 13.83 91 164493 20.15 ug/l 98 90) Hexachloroethane 14.10 117 33128 21.43 ug/l 96 91) 1,2-Dichlorobenzene 13.88 146 92140 21.72 ug/l 99 92) 1,2-Dibromo-3-Chloropropan 14.49 75 7491 23.13 ug/l 95 93) 1,2,4-Trichlorobenzene 15.15 180 64030 20.73 ug/l 99 94) Hexachlorobutadiene 15.25 225 35651 20.74 ug/l 98 95) Naphthalene 15.38 128 122668 21.84 ug/l 99 96) 1,2,3-Trichlorobenzene 15.57 180 61580 22.28 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed