Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052518\ Quantitation Report (QT Reviewed) Data File : VW002861.D Acq On : 24 May 2018 23:41 Operator : JC/SY Sample : VW0525SBSD01 Misc : 5.00G/5ML/MSVOA_W/SOIL ALS Vial : 31 Sample Multiplier: 1 Quant Time: May 25 09:01:03 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\82W051518S.M Quant Title : SW846 8260 QLast Update : Tue May 15 03:32:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 7.95 168 185000 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 8.85 114 289932 50.00 ug/l 0.00 63) Chlorobenzene-d5 11.64 117 275326 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 13.57 152 152066 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 8.31 65 110846 57.98 ug/l 0.00 Spiked Amount 50.000 Recovery = 115.96% 35) Dibromofluoromethane 7.88 113 96266 52.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.68% 50) Toluene-d8 10.33 98 364392 52.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.14% 62) 4-Bromofluorobenzene 12.63 95 133584 52.20 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.40% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 12667 17.74 ug/l 96 3) Chloromethane 2.21 50 29646 21.71 ug/l 99 4) Vinyl Chloride 2.35 62 44791 20.92 ug/l 97 5) Bromomethane 2.76 94 36305 20.68 ug/l 96 6) Chloroethane 2.91 64 30647 20.80 ug/l 98 7) Trichlorofluoromethane 3.24 101 13579 14.39 ug/l 97 8) Diethyl Ether 3.67 74 29425 26.06 ug/l 98 9) 1,1,2-Trichlorotrifluoroet 4.04 101 33141 21.20 ug/l 99 10) Methyl Iodide 4.26 142 51017 20.48 ug/l 98 11) Tert butyl alcohol 5.20 59 16745 113.95 ug/l 97 12) 1,1-Dichloroethene 4.03 96 32561 21.04 ug/l 93 13) Acrolein 3.88 56 10668 73.69 ug/l 91 14) Allyl chloride 4.65 41 39438 17.18 ug/l 96 15) Acrylonitrile 5.36 53 46071 113.15 ug/l 99 16) Acetone 4.12 43 43112 106.82 ug/l 98 17) Carbon Disulfide 4.37 76 85400 20.06 ug/l 100 18) Methyl Acetate 4.67 43 27632 23.49 ug/l 98 19) Methyl tert-butyl Ether 5.43 73 63463 22.32 ug/l 97 20) Methylene Chloride 4.91 84 39742 23.28 ug/l 96 21) trans-1,2-Dichloroethene 5.40 96 35716 21.35 ug/l 94 22) Diisopropyl ether 6.31 45 112244 22.07 ug/l 99 23) Vinyl Acetate 6.26 43 339354 110.09 ug/l 100 24) 1,1-Dichloroethane 6.20 63 67007 21.86 ug/l 99 25) 2-Butanone 7.18 43 68691 120.36 ug/l 95 26) 2,2-Dichloropropane 7.15 77 28996 16.88 ug/l 100 27) cis-1,2-Dichloroethene 7.17 96 40854 21.41 ug/l 98 28) Bromochloromethane 7.51 49 33116 24.20 ug/l 96 29) Tetrahydrofuran 7.53 42 43517 122.06 ug/l 98 30) Chloroform 7.67 83 72762 22.23 ug/l 98 31) Cyclohexane 7.95 56 51812 19.08 ug/l # 95 32) 1,1,1-Trichloroethane 7.87 97 50976 20.65 ug/l 98 36) 1,1-Dichloropropene 8.08 75 50889 19.89 ug/l 98 37) Ethyl Acetate 7.26 43 29634 23.35 ug/l 98 38) Carbon Tetrachloride 8.06 117 48906 19.52 ug/l 99 39) Methylcyclohexane 9.34 83 55191 18.83 ug/l 94 40) Benzene 8.32 78 153924 20.95 ug/l 96 41) Methacrylonitrile 7.49 41 16903 23.80 ug/l 93 42) 1,2-Dichloroethane 8.40 62 51624 22.13 ug/l 99 43) Isopropyl Acetate 8.43 43 55833 22.88 ug/l 100 44) Trichloroethene 9.10 130 40412 20.07 ug/l 93 45) 1,2-Dichloropropane 9.37 63 40135 21.44 ug/l 99 46) Dibromomethane 9.46 93 23442 22.01 ug/l 98 47) Bromodichloromethane 9.65 83 52824 21.26 ug/l 97 48) Methyl methacrylate 9.45 41 28097 23.76 ug/l 94 49) 1,4-Dioxane 9.45 88 8304 467.79 ug/l 96 51) 4-Methyl-2-Pentanone 10.22 43 154434 115.25 ug/l 99 52) Toluene 10.39 92 98812 21.27 ug/l 99 53) t-1,3-Dichloropropene 10.61 75 49518 19.71 ug/l 93 54) cis-1,3-Dichloropropene 10.08 75 57566 20.56 ug/l 99 55) 1,1,2-Trichloroethane 10.79 97 33638 22.41 ug/l 97 56) Ethyl methacrylate 10.65 69 39615 21.66 ug/l 99 57) 1,3-Dichloropropane 10.94 76 55018 22.10 ug/l 98 58) 2-Chloroethyl Vinyl ether 9.93 63 103530 115.32 ug/l 99 59) 2-Hexanone 10.98 43 107520 116.22 ug/l 98 60) Dibromochloromethane 11.13 129 38046 21.49 ug/l 97 61) 1,2-Dibromoethane 11.24 107 32047 22.13 ug/l 99 64) Tetrachloroethene 10.87 164 46413 23.92 ug/l 98 65) Chlorobenzene 11.66 112 111725 20.37 ug/l 99 66) 1,1,1,2-Tetrachloroethane 11.74 131 40672 20.72 ug/l 99 67) Ethyl Benzene 11.74 91 185059 19.86 ug/l 97 68) m/p-Xylenes 11.85 106 143987 39.74 ug/l 100 69) o-Xylene 12.18 106 68320 19.84 ug/l 100 70) Styrene 12.19 104 116483 20.33 ug/l 99 71) Bromoform 12.36 173 23817 20.65 ug/l # 99 73) Isopropylbenzene 12.48 105 181074 19.32 ug/l 100 74) N-amyl acetate 12.28 43 52610 22.03 ug/l 98 75) 1,1,2,2-Tetrachloroethane 12.73 83 41320 21.76 ug/l 99 76) 1,2,3-Trichloropropane 12.77 75 30857m 21.47 ug/l 77) Bromobenzene 12.76 156 48985 20.48 ug/l 99 78) n-propylbenzene 12.81 91 224933 19.87 ug/l 100 79) 2-Chlorotoluene 12.90 91 130265 20.26 ug/l 99 80) 1,3,5-Trimethylbenzene 12.95 105 160376 20.05 ug/l 99 81) trans-1,4-Dichloro-2-buten 12.52 75 10270 19.48 ug/l 96 82) 4-Chlorotoluene 13.00 91 140326 20.19 ug/l 99 83) tert-Butylbenzene 13.21 119 134338 19.45 ug/l 98 84) 1,2,4-Trimethylbenzene 13.26 105 165539 19.93 ug/l 98 85) sec-Butylbenzene 13.40 105 195279 19.67 ug/l 99 86) p-Isopropyltoluene 13.51 119 172941 19.37 ug/l 99 87) 1,3-Dichlorobenzene 13.51 146 98362 20.33 ug/l 99 88) 1,4-Dichlorobenzene 13.59 146 97155 20.19 ug/l 99 89) n-Butylbenzene 13.83 91 160136 18.96 ug/l 99 90) Hexachloroethane 14.10 117 31489 19.70 ug/l 98 91) 1,2-Dichlorobenzene 13.88 146 91528 20.85 ug/l 100 92) 1,2-Dibromo-3-Chloropropan 14.50 75 7643 22.81 ug/l 96 93) 1,2,4-Trichlorobenzene 15.15 180 64597 20.22 ug/l 99 94) Hexachlorobutadiene 15.25 225 35756 20.11 ug/l 99 95) Naphthalene 15.38 128 124439 21.42 ug/l 100 96) 1,2,3-Trichlorobenzene 15.57 180 61070 21.36 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed