Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052518\ Quantitation Report (QT Reviewed) Data File : VW002868.D Acq On : 25 May 2018 12:38 Operator : JC/SY Sample : VSTDCCC050 Misc : 5.00G/5ML/MSVOA_W/SOIL ALS Vial : 2 Sample Multiplier: 1 Quant Time: May 26 05:36:06 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\82W051518S.M Quant Title : SW846 8260 QLast Update : Tue May 15 03:32:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 7.95 168 230291 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 8.85 114 338327 50.00 ug/l 0.00 63) Chlorobenzene-d5 11.64 117 310331 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 13.57 152 168986 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 8.31 65 115455 48.52 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.04% 35) Dibromofluoromethane 7.88 113 109265 50.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.82% 50) Toluene-d8 10.33 98 423680 51.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.76% 62) 4-Bromofluorobenzene 12.63 95 152494 51.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.14% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 40847m 45.97 ug/l 3) Chloromethane 2.21 50 74953 44.09 ug/l 95 4) Vinyl Chloride 2.36 62 120991 45.39 ug/l 98 5) Bromomethane 2.77 94 88696 40.58 ug/l 99 6) Chloroethane 2.92 64 75993 41.43 ug/l 96 7) Trichlorofluoromethane 3.25 101 68713 58.50 ug/l 98 8) Diethyl Ether 3.67 74 50406 35.86 ug/l 95 9) 1,1,2-Trichlorotrifluoroet 4.05 101 99986 51.38 ug/l 99 10) Methyl Iodide 4.26 142 142927 46.09 ug/l 97 11) Tert butyl alcohol 5.17 59 38631 211.18 ug/l 99 12) 1,1-Dichloroethene 4.03 96 94229 48.92 ug/l 94 13) Acrolein 3.89 56 47866 265.61 ug/l 99 14) Allyl chloride 4.65 41 148947 52.11 ug/l 99 15) Acrylonitrile 5.36 53 112675 222.30 ug/l 99 16) Acetone 4.11 43 144733 288.08 ug/l 99 17) Carbon Disulfide 4.37 76 240841 45.44 ug/l 99 18) Methyl Acetate 4.66 43 67566 46.13 ug/l 98 19) Methyl tert-butyl Ether 5.42 73 169763 47.97 ug/l 98 20) Methylene Chloride 4.90 84 102110 51.15 ug/l 96 21) trans-1,2-Dichloroethene 5.41 96 99895 47.98 ug/l 98 22) Diisopropyl ether 6.31 45 311699 49.23 ug/l 98 23) Vinyl Acetate 6.25 43 919988 239.75 ug/l 100 24) 1,1-Dichloroethane 6.21 63 189540 49.67 ug/l 98 25) 2-Butanone 7.17 43 166981 235.03 ug/l 99 26) 2,2-Dichloropropane 7.17 77 120781 56.48 ug/l 96 27) cis-1,2-Dichloroethene 7.17 96 113678 47.85 ug/l 96 28) Bromochloromethane 7.51 49 84120 49.38 ug/l 96 29) Tetrahydrofuran 7.52 42 96592 217.65 ug/l 99 30) Chloroform 7.67 83 198466 48.71 ug/l 94 31) Cyclohexane 7.95 56 161109 47.66 ug/l 98 32) 1,1,1-Trichloroethane 7.87 97 157168 51.14 ug/l 99 36) 1,1-Dichloropropene 8.08 75 150306 50.34 ug/l 99 37) Ethyl Acetate 7.25 43 65813 44.45 ug/l 98 38) Carbon Tetrachloride 8.07 117 153243 52.42 ug/l 97 39) Methylcyclohexane 9.34 83 176042 51.48 ug/l 99 40) Benzene 8.32 78 425219 49.60 ug/l 98 41) Methacrylonitrile 7.48 41 33903 40.91 ug/l 95 42) 1,2-Dichloroethane 8.40 62 131869 48.44 ug/l 99 43) Isopropyl Acetate 8.43 43 129358 45.42 ug/l 99 44) Trichloroethene 9.09 130 116372 49.54 ug/l 96 45) 1,2-Dichloropropane 9.37 63 108160 49.52 ug/l 100 46) Dibromomethane 9.46 93 57251 46.06 ug/l 99 47) Bromodichloromethane 9.65 83 145906 50.33 ug/l 99 48) Methyl methacrylate 9.44 41 61616 44.65 ug/l 99 49) 1,4-Dioxane 9.45 88 18525 894.29 ug/l 98 51) 4-Methyl-2-Pentanone 10.21 43 352459 225.40 ug/l 99 52) Toluene 10.39 92 274508 50.65 ug/l 100 53) t-1,3-Dichloropropene 10.61 75 148951 50.82 ug/l 97 54) cis-1,3-Dichloropropene 10.08 75 167023 51.11 ug/l 98 55) 1,1,2-Trichloroethane 10.79 97 82607 47.17 ug/l 99 56) Ethyl methacrylate 10.65 69 101164 47.41 ug/l 100 57) 1,3-Dichloropropane 10.94 76 141282 48.64 ug/l 100 58) 2-Chloroethyl Vinyl ether 9.93 63 258789 247.02 ug/l 99 59) 2-Hexanone 10.98 43 255247 236.44 ug/l 98 60) Dibromochloromethane 11.13 129 100982 48.87 ug/l 99 61) 1,2-Dibromoethane 11.24 107 78843 46.65 ug/l 98 64) Tetrachloroethene 10.87 164 99565 45.52 ug/l 98 65) Chlorobenzene 11.66 112 307705 49.78 ug/l 97 66) 1,1,1,2-Tetrachloroethane 11.74 131 112153 50.69 ug/l 100 67) Ethyl Benzene 11.74 91 547039 52.08 ug/l 99 68) m/p-Xylenes 11.85 106 424883 104.03 ug/l 100 69) o-Xylene 12.18 106 198573 51.17 ug/l 100 70) Styrene 12.19 104 333569 51.65 ug/l 100 71) Bromoform 12.35 173 62234 47.87 ug/l # 98 73) Isopropylbenzene 12.48 105 567168 54.45 ug/l 99 74) N-amyl acetate 12.28 43 125850 47.43 ug/l 98 75) 1,1,2,2-Tetrachloroethane 12.73 83 100892 47.80 ug/l 99 76) 1,2,3-Trichloropropane 12.77 75 74202m 46.45 ug/l 77) Bromobenzene 12.76 156 133397 50.19 ug/l 99 78) n-propylbenzene 12.81 91 686084 54.54 ug/l 99 79) 2-Chlorotoluene 12.90 91 383426 53.67 ug/l 99 80) 1,3,5-Trimethylbenzene 12.95 105 482470 54.27 ug/l 99 81) trans-1,4-Dichloro-2-buten 12.52 75 30291 51.70 ug/l 97 82) 4-Chlorotoluene 13.00 91 406782 52.66 ug/l 99 83) tert-Butylbenzene 13.21 119 426854 55.60 ug/l 100 84) 1,2,4-Trimethylbenzene 13.26 105 494588 53.60 ug/l 99 85) sec-Butylbenzene 13.40 105 610258 55.33 ug/l 100 86) p-Isopropyltoluene 13.51 119 545641 55.00 ug/l 99 87) 1,3-Dichlorobenzene 13.51 146 274051 50.98 ug/l 100 88) 1,4-Dichlorobenzene 13.58 146 270347 50.55 ug/l 99 89) n-Butylbenzene 13.83 91 526289 56.08 ug/l 99 90) Hexachloroethane 14.10 117 95417 53.70 ug/l 99 91) 1,2-Dichlorobenzene 13.88 146 244116 50.05 ug/l 99 92) 1,2-Dibromo-3-Chloropropan 14.49 75 16976 45.59 ug/l 95 93) 1,2,4-Trichlorobenzene 15.15 180 177980 50.12 ug/l 99 94) Hexachlorobutadiene 15.25 225 105359 53.32 ug/l 99 95) Naphthalene 15.38 128 306483 47.47 ug/l 99 96) 1,2,3-Trichlorobenzene 15.57 180 153518 48.32 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed