Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052518\ Quantitation Report (QT Reviewed) Data File : VW002870.D Acq On : 25 May 2018 13:57 Operator : JC/SY Sample : VW0525SBS02 Misc : 5.00G/5ML/MSVOA_W/SOIL ALS Vial : 4 Sample Multiplier: 1 Quant Time: May 25 15:19:46 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\82W051518S.M Quant Title : SW846 8260 QLast Update : Tue May 15 03:32:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 7.95 168 213985 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 8.85 114 315477 50.00 ug/l 0.00 63) Chlorobenzene-d5 11.64 117 288835 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 13.57 152 157135 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 8.31 65 110817 50.12 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.24% 35) Dibromofluoromethane 7.88 113 100893 50.41 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.82% 50) Toluene-d8 10.33 98 395269 51.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.82% 62) 4-Bromofluorobenzene 12.63 95 141610 50.86 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.72% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.00 85 11638 14.09 ug/l 88 3) Chloromethane 2.21 50 31615 20.02 ug/l 98 4) Vinyl Chloride 2.36 62 46742 18.87 ug/l 100 5) Bromomethane 2.77 94 38475 18.95 ug/l 95 6) Chloroethane 2.92 64 32667 19.17 ug/l 94 7) Trichlorofluoromethane 3.25 101 28132 25.78 ug/l 92 8) Diethyl Ether 3.67 74 20905 16.01 ug/l 99 9) 1,1,2-Trichlorotrifluoroet 4.05 101 41160 22.76 ug/l 98 10) Methyl Iodide 4.26 142 61281 21.27 ug/l 98 11) Tert butyl alcohol 5.18 59 15605m 91.81 ug/l 12) 1,1-Dichloroethene 4.03 96 39986 22.34 ug/l 92 13) Acrolein 3.89 56 12627 75.41 ug/l 93 14) Allyl chloride 4.65 41 59176 22.28 ug/l 96 15) Acrylonitrile 5.36 53 46220 98.14 ug/l 98 16) Acetone 4.12 43 59927 128.37 ug/l 97 17) Carbon Disulfide 4.37 76 108393 22.01 ug/l 100 18) Methyl Acetate 4.67 43 23972 17.61 ug/l 96 19) Methyl tert-butyl Ether 5.43 73 67734 20.60 ug/l 95 20) Methylene Chloride 4.90 84 47488 24.15 ug/l 95 21) trans-1,2-Dichloroethene 5.41 96 41405 21.40 ug/l 100 22) Diisopropyl ether 6.31 45 123846 21.05 ug/l 97 23) Vinyl Acetate 6.25 43 367357 103.03 ug/l 99 24) 1,1-Dichloroethane 6.21 63 77593 21.88 ug/l 98 25) 2-Butanone 7.17 43 66567 100.84 ug/l 94 26) 2,2-Dichloropropane 7.17 77 52196 26.27 ug/l 97 27) cis-1,2-Dichloroethene 7.17 96 45243 20.50 ug/l 94 28) Bromochloromethane 7.51 49 34058 21.52 ug/l 97 29) Tetrahydrofuran 7.53 42 36055 87.43 ug/l 98 30) Chloroform 7.67 83 80827 21.35 ug/l 99 31) Cyclohexane 7.95 56 68656 21.86 ug/l 95 32) 1,1,1-Trichloroethane 7.87 97 65584 22.97 ug/l 100 36) 1,1-Dichloropropene 8.08 75 62789 22.55 ug/l 97 37) Ethyl Acetate 7.26 43 26864 19.46 ug/l 98 38) Carbon Tetrachloride 8.07 117 62931 23.09 ug/l 99 39) Methylcyclohexane 9.34 83 70012 21.96 ug/l 96 40) Benzene 8.32 78 175884 22.00 ug/l 99 41) Methacrylonitrile 7.48 41 15852 20.51 ug/l # 90 42) 1,2-Dichloroethane 8.40 62 52745 20.78 ug/l 100 43) Isopropyl Acetate 8.43 43 50884 19.16 ug/l 98 44) Trichloroethene 9.10 130 48006 21.92 ug/l 93 45) 1,2-Dichloropropane 9.37 63 44441 21.82 ug/l 98 46) Dibromomethane 9.46 93 24005 20.71 ug/l 97 47) Bromodichloromethane 9.65 83 56796 21.01 ug/l 98 48) Methyl methacrylate 9.45 41 23249 18.07 ug/l 97 49) 1,4-Dioxane 9.46 88 6387 330.66 ug/l 96 51) 4-Methyl-2-Pentanone 10.22 43 132605 90.95 ug/l 99 52) Toluene 10.39 92 112975 22.35 ug/l 99 53) t-1,3-Dichloropropene 10.61 75 57058 20.88 ug/l 98 54) cis-1,3-Dichloropropene 10.08 75 66326 21.77 ug/l 99 55) 1,1,2-Trichloroethane 10.79 97 32917 20.16 ug/l 98 56) Ethyl methacrylate 10.65 69 36955 18.57 ug/l 99 57) 1,3-Dichloropropane 10.94 76 55998 20.68 ug/l 100 58) 2-Chloroethyl Vinyl ether 9.93 63 97763 100.08 ug/l 100 59) 2-Hexanone 10.98 43 98356 97.71 ug/l 98 60) Dibromochloromethane 11.13 129 38882 20.18 ug/l 99 61) 1,2-Dibromoethane 11.24 107 31866 20.22 ug/l 99 64) Tetrachloroethene 10.87 164 41681 20.47 ug/l 92 65) Chlorobenzene 11.66 112 126614 22.01 ug/l 97 66) 1,1,1,2-Tetrachloroethane 11.74 131 45092 21.90 ug/l 96 67) Ethyl Benzene 11.74 91 215700 22.06 ug/l 99 68) m/p-Xylenes 11.85 106 169625 44.62 ug/l 98 69) o-Xylene 12.18 106 77406 21.43 ug/l 100 70) Styrene 12.19 104 127999 21.29 ug/l 99 71) Bromoform 12.36 173 23936 19.78 ug/l # 99 73) Isopropylbenzene 12.48 105 215772 22.28 ug/l 99 74) N-amyl acetate 12.28 43 47246 19.15 ug/l 97 75) 1,1,2,2-Tetrachloroethane 12.72 83 39248 20.00 ug/l 99 76) 1,2,3-Trichloropropane 12.77 75 28389m 19.11 ug/l 77) Bromobenzene 12.76 156 53842 21.79 ug/l 97 78) n-propylbenzene 12.81 91 264610 22.62 ug/l 100 79) 2-Chlorotoluene 12.90 91 150336 22.63 ug/l 99 80) 1,3,5-Trimethylbenzene 12.95 105 183539 22.20 ug/l 99 81) trans-1,4-Dichloro-2-buten 12.52 75 10997 20.19 ug/l 95 82) 4-Chlorotoluene 13.00 91 160127 22.29 ug/l 99 83) tert-Butylbenzene 13.22 119 161447 22.62 ug/l 98 84) 1,2,4-Trimethylbenzene 13.26 105 190170 22.16 ug/l 100 85) sec-Butylbenzene 13.40 105 233291 22.75 ug/l 100 86) p-Isopropyltoluene 13.51 119 205625 22.29 ug/l 98 87) 1,3-Dichlorobenzene 13.51 146 107496 21.50 ug/l 100 88) 1,4-Dichlorobenzene 13.59 146 108345 21.79 ug/l 99 89) n-Butylbenzene 13.83 91 199701 22.88 ug/l 99 90) Hexachloroethane 14.10 117 37648 22.79 ug/l 95 91) 1,2-Dichlorobenzene 13.88 146 96907 21.37 ug/l 99 92) 1,2-Dibromo-3-Chloropropan 14.50 75 6708 19.37 ug/l 91 93) 1,2,4-Trichlorobenzene 15.15 180 69651 21.10 ug/l 98 94) Hexachlorobutadiene 15.25 225 42264 23.00 ug/l 98 95) Naphthalene 15.38 128 114280 19.04 ug/l 100 96) 1,2,3-Trichlorobenzene 15.57 180 61766 20.91 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed