Data Path : W:\HPCHEM1\MSVOA_W\DATA\VW052518\ Quantitation Report (QT Reviewed) Data File : VW002871.D Acq On : 25 May 2018 14:23 Operator : JC/SY Sample : VW0525SBSD02 Misc : 5.00G/5ML/MSVOA_W/SOIL ALS Vial : 5 Sample Multiplier: 1 Quant Time: May 25 15:18:47 2018 Quant Method : W:\HPCHEM1\MSVOA_W\METHOD\82W051518S.M Quant Title : SW846 8260 QLast Update : Tue May 15 03:32:11 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 7.95 168 227698 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 8.85 114 333520 50.00 ug/l 0.00 63) Chlorobenzene-d5 11.64 117 304533 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 13.57 152 166830 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 8.31 65 124221 52.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.58% 35) Dibromofluoromethane 7.88 113 116330 54.98 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.96% 50) Toluene-d8 10.33 98 451027 56.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.06% 62) 4-Bromofluorobenzene 12.63 95 161006 54.70 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.40% Target Compounds Qvalue 2) Dichlorodifluoromethane 2.01 85 11290 12.85 ug/l 98 3) Chloromethane 2.21 50 31705 18.86 ug/l 96 4) Vinyl Chloride 2.36 62 49493 18.78 ug/l 94 5) Bromomethane 2.77 94 39794 18.41 ug/l 93 6) Chloroethane 2.92 64 34432 18.98 ug/l 97 7) Trichlorofluoromethane 3.25 101 29182 25.13 ug/l 100 8) Diethyl Ether 3.67 74 22482 16.18 ug/l 100 9) 1,1,2-Trichlorotrifluoroet 4.05 101 42332 22.00 ug/l 98 10) Methyl Iodide 4.26 142 63775 20.80 ug/l 98 11) Tert butyl alcohol 5.19 59 15859 87.68 ug/l # 85 12) 1,1-Dichloroethene 4.03 96 40095 21.05 ug/l 97 13) Acrolein 3.89 56 12851 72.12 ug/l 97 14) Allyl chloride 4.66 41 62677 22.18 ug/l 97 15) Acrylonitrile 5.37 53 46174 92.14 ug/l 97 16) Acetone 4.12 43 59417 119.61 ug/l 97 17) Carbon Disulfide 4.37 76 108019 20.61 ug/l 97 18) Methyl Acetate 4.67 43 24924 17.21 ug/l 98 19) Methyl tert-butyl Ether 5.43 73 71193 20.34 ug/l 98 20) Methylene Chloride 4.90 84 48590 23.11 ug/l 98 21) trans-1,2-Dichloroethene 5.42 96 43864 21.31 ug/l 92 22) Diisopropyl ether 6.31 45 130957 20.92 ug/l 97 23) Vinyl Acetate 6.26 43 382301 100.76 ug/l 99 24) 1,1-Dichloroethane 6.21 63 81563 21.62 ug/l 97 25) 2-Butanone 7.18 43 68756 97.88 ug/l 96 26) 2,2-Dichloropropane 7.17 77 51923 24.56 ug/l 98 27) cis-1,2-Dichloroethene 7.17 96 47997 20.43 ug/l 96 28) Bromochloromethane 7.51 49 35687 21.19 ug/l 100 29) Tetrahydrofuran 7.54 42 40635 92.60 ug/l 95 30) Chloroform 7.68 83 83906 20.83 ug/l 97 31) Cyclohexane 7.95 56 70857 21.20 ug/l 97 32) 1,1,1-Trichloroethane 7.87 97 67480 22.21 ug/l 99 36) 1,1-Dichloropropene 8.09 75 66618 22.63 ug/l 98 37) Ethyl Acetate 7.26 43 29430 20.16 ug/l 99 38) Carbon Tetrachloride 8.07 117 65092 22.59 ug/l 96 39) Methylcyclohexane 9.34 83 74211 22.01 ug/l 99 40) Benzene 8.32 78 183151 21.67 ug/l 93 41) Methacrylonitrile 7.49 41 16660 20.39 ug/l 96 42) 1,2-Dichloroethane 8.40 62 57119 21.28 ug/l 100 43) Isopropyl Acetate 8.43 43 54759 19.50 ug/l 99 44) Trichloroethene 9.10 130 49499 21.38 ug/l 100 45) 1,2-Dichloropropane 9.37 63 45295 21.04 ug/l 97 46) Dibromomethane 9.46 93 24993 20.40 ug/l 99 47) Bromodichloromethane 9.65 83 59418 20.79 ug/l 98 48) Methyl methacrylate 9.44 41 25012 18.39 ug/l 97 49) 1,4-Dioxane 9.46 88 6520 319.29 ug/l 99 51) 4-Methyl-2-Pentanone 10.22 43 140710 91.28 ug/l 98 52) Toluene 10.40 92 118532 22.19 ug/l 100 53) t-1,3-Dichloropropene 10.61 75 59670 20.65 ug/l 97 54) cis-1,3-Dichloropropene 10.08 75 67948 21.09 ug/l 98 55) 1,1,2-Trichloroethane 10.79 97 35131 20.35 ug/l 97 56) Ethyl methacrylate 10.65 69 39593 18.82 ug/l 98 57) 1,3-Dichloropropane 10.94 76 57786 20.18 ug/l 98 58) 2-Chloroethyl Vinyl ether 9.93 63 102904 99.64 ug/l 100 59) 2-Hexanone 10.98 43 102281 96.11 ug/l 98 60) Dibromochloromethane 11.13 129 40833 20.05 ug/l 100 61) 1,2-Dibromoethane 11.24 107 32304 19.39 ug/l 95 64) Tetrachloroethene 10.87 164 42370 19.74 ug/l 98 65) Chlorobenzene 11.66 112 131049 21.61 ug/l 99 66) 1,1,1,2-Tetrachloroethane 11.74 131 46316 21.33 ug/l 98 67) Ethyl Benzene 11.74 91 225202 21.85 ug/l 98 68) m/p-Xylenes 11.85 106 174867 43.63 ug/l 99 69) o-Xylene 12.18 106 81784 21.47 ug/l 97 70) Styrene 12.19 104 134470 21.22 ug/l 99 71) Bromoform 12.35 173 24829 19.46 ug/l # 100 73) Isopropylbenzene 12.48 105 225822 21.96 ug/l 99 74) N-amyl acetate 12.28 43 49386 18.85 ug/l 98 75) 1,1,2,2-Tetrachloroethane 12.72 83 41543 19.94 ug/l 99 76) 1,2,3-Trichloropropane 12.77 75 29277m 18.57 ug/l 77) Bromobenzene 12.76 156 55241 21.05 ug/l 98 78) n-propylbenzene 12.81 91 281500 22.67 ug/l 100 79) 2-Chlorotoluene 12.90 91 157308 22.30 ug/l 99 80) 1,3,5-Trimethylbenzene 12.95 105 195126 22.23 ug/l 99 81) trans-1,4-Dichloro-2-buten 12.52 75 11501 19.88 ug/l 94 82) 4-Chlorotoluene 13.00 91 165379 21.69 ug/l 99 83) tert-Butylbenzene 13.22 119 170687 22.52 ug/l 99 84) 1,2,4-Trimethylbenzene 13.26 105 199865 21.94 ug/l 99 85) sec-Butylbenzene 13.40 105 245226 22.52 ug/l 100 86) p-Isopropyltoluene 13.51 119 219967 22.46 ug/l 99 87) 1,3-Dichlorobenzene 13.51 146 115295 21.72 ug/l 99 88) 1,4-Dichlorobenzene 13.59 146 114621 21.71 ug/l 99 89) n-Butylbenzene 13.83 91 208963 22.55 ug/l 99 90) Hexachloroethane 14.10 117 38294 21.83 ug/l 98 91) 1,2-Dichlorobenzene 13.88 146 101198 21.02 ug/l 100 92) 1,2-Dibromo-3-Chloropropan 14.50 75 6746 18.35 ug/l 96 93) 1,2,4-Trichlorobenzene 15.15 180 74447 21.24 ug/l 99 94) Hexachlorobutadiene 15.25 225 43652 22.38 ug/l 99 95) Naphthalene 15.38 128 119954 18.82 ug/l 99 96) 1,2,3-Trichlorobenzene 15.57 180 64033 20.41 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed