Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001506.D Acq On : 08 May 2018 11:46 Operator : JC/MD Sample : J2695-08 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 4 Sample Multiplier: 1 Quant Time: May 08 14:12:52 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 261937 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 358353 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 326607 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 196556 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 175130 46.52 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.04% 35) Dibromofluoromethane 5.51 113 136120 42.70 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.40% 50) Toluene-d8 8.72 98 514828 44.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.50% 62) 4-Bromofluorobenzene 11.14 95 178244 39.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 79.82% Target Compounds Qvalue 11) Tert butyl alcohol 3.07 59 7322 9.22 ug/l 98 16) Acetone 2.45 43 509590 298.09 ug/l 99 17) Carbon Disulfide 2.57 76 10583 1.43 ug/l 98 25) 2-Butanone 4.71 43 218764 88.53 ug/l 98 30) Chloroform 5.22 83 15331 2.64 ug/l 97 40) Benzene 6.15 78 4628 0.35 ug/l 97 51) 4-Methyl-2-Pentanone 8.65 43 178879 35.09 ug/l 99 52) Toluene 8.79 92 10079 1.16 ug/l 99 59) 2-Hexanone 9.50 43 23889 6.12 ug/l 100 67) Ethyl Benzene 10.26 91 3879 0.25 ug/l 99 68) m/p-Xylenes 10.36 106 5769 0.93 ug/l 95 69) o-Xylene 10.70 106 2914 0.48 ug/l 98 84) 1,2,4-Trimethylbenzene 11.81 105 8093 0.70 ug/l 92 86) p-Isopropyltoluene 12.07 119 3460 0.28 ug/l # 71 95) Naphthalene 13.84 128 5300 0.36 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed