Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001508.D Acq On : 08 May 2018 12:39 Operator : JC/MD Sample : J2659-09 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 5 Sample Multiplier: 1 Quant Time: May 09 06:57:20 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 282314 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 384750 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 343859 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 204933 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 225197 55.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.00% 35) Dibromofluoromethane 5.51 113 175883 51.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.78% 50) Toluene-d8 8.72 98 648430 51.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.82% 62) 4-Bromofluorobenzene 11.14 95 224684 46.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.70% Target Compounds Qvalue 16) Acetone 2.45 43 10394 5.64 ug/l 95 44) Trichloroethene 7.22 130 10934 2.50 ug/l 96 64) Tetrachloroethene 9.34 164 1634 0.34 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed