Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001509.D Acq On : 08 May 2018 13:06 Operator : JC/MD Sample : J2659-10 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 5 Sample Multiplier: 1 Quant Time: May 09 06:59:46 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 274261 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 375027 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 329229 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 182738 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 223347 56.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 113.32% 35) Dibromofluoromethane 5.51 113 174512 52.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.62% 50) Toluene-d8 8.72 98 638244 52.42 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.84% 62) 4-Bromofluorobenzene 11.14 95 211645 45.28 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.56% Target Compounds Qvalue 16) Acetone 2.45 43 8752 4.89 ug/l 93 24) 1,1-Dichloroethane 3.70 63 9342 1.58 ug/l 97 44) Trichloroethene 7.22 130 17149 4.03 ug/l 99 64) Tetrachloroethene 9.34 164 3098 0.68 ug/l 88 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed