Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001512.D Acq On : 08 May 2018 14:26 Operator : JC/MD Sample : J2659-18 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 6 Sample Multiplier: 1 Quant Time: May 09 07:04:18 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 273209 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 378118 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 344536 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 208753 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 226709 57.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 115.46% 35) Dibromofluoromethane 5.51 113 176288 52.42 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.84% 50) Toluene-d8 8.72 98 643016 52.38 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.76% 62) 4-Bromofluorobenzene 11.14 95 224653 47.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.34% Target Compounds Qvalue 16) Acetone 2.45 43 9564 5.36 ug/l 93 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed