Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001513.D Acq On : 08 May 2018 14:53 Operator : JC/MD Sample : J2659-19 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 7 Sample Multiplier: 1 Quant Time: May 09 07:05:44 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 267312 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 367624 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 336552 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 210629 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 223367 58.14 ug/l 0.00 Spiked Amount 50.000 Recovery = 116.28% 35) Dibromofluoromethane 5.51 113 171553 52.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.92% 50) Toluene-d8 8.72 98 634320 53.14 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.28% 62) 4-Bromofluorobenzene 11.14 95 224917 49.09 ug/l 0.00 Spiked Amount 50.000 Recovery = 98.18% Target Compounds Qvalue 16) Acetone 2.45 43 8592 4.92 ug/l 93 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed