Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001515.D Acq On : 08 May 2018 15:46 Operator : JC/MD Sample : J2659-21 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 9 Sample Multiplier: 1 Quant Time: May 09 07:12:35 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 258906 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 358091 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 317058 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 178814 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 215976 58.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 116.08% 35) Dibromofluoromethane 5.51 113 164977 51.80 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.60% 50) Toluene-d8 8.72 98 593797 51.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.14% 62) 4-Bromofluorobenzene 11.14 95 197766 44.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.62% Target Compounds Qvalue 16) Acetone 2.45 43 7291 4.31 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed