Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001516.D Acq On : 08 May 2018 16:13 Operator : JC/MD Sample : J2659-22RE Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 10 Sample Multiplier: 1 Quant Time: May 09 07:14:08 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 252561 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 347972 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 308100 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 172991 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 217755 59.99 ug/l 0.00 Spiked Amount 50.000 Recovery = 119.98% 35) Dibromofluoromethane 5.51 113 167868 54.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.48% 50) Toluene-d8 8.72 98 587881 52.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.06% 62) 4-Bromofluorobenzene 11.14 95 196292 45.26 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.52% Target Compounds Qvalue 16) Acetone 2.45 43 6999 4.25 ug/l # 79 19) Methyl tert-butyl Ether 3.21 73 23451 2.41 ug/l 94 27) cis-1,2-Dichloroethene 4.60 96 23624 7.11 ug/l 88 30) Chloroform 5.22 83 8199 1.46 ug/l 96 44) Trichloroethene 7.22 130 8746 2.21 ug/l 90 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed