Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001517.D Acq On : 08 May 2018 16:40 Operator : JC/MD Sample : J2787-01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 11 Sample Multiplier: 1 Quant Time: May 09 07:16:18 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 242363 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 326102 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 293982 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 168900 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 161172 46.27 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.54% 35) Dibromofluoromethane 5.51 113 127929 44.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 88.20% 50) Toluene-d8 8.72 98 452934 42.78 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.56% 62) 4-Bromofluorobenzene 11.14 95 156208 38.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 76.86% Target Compounds Qvalue 11) Tert butyl alcohol 3.08 59 8789 11.97 ug/l 96 16) Acetone 2.45 43 78308 49.51 ug/l 99 25) 2-Butanone 4.72 43 54621 23.89 ug/l 96 29) Tetrahydrofuran 5.18 42 214069 146.33 ug/l 99 51) 4-Methyl-2-Pentanone 8.66 43 11438 2.47 ug/l 98 52) Toluene 8.79 92 161076 20.33 ug/l 98 67) Ethyl Benzene 10.26 91 3818 0.27 ug/l 97 68) m/p-Xylenes 10.36 106 2908 0.52 ug/l 96 69) o-Xylene 10.70 106 22602 4.16 ug/l 96 73) Isopropylbenzene 11.02 105 15580 1.33 ug/l 98 78) n-propylbenzene 11.37 91 7368 0.58 ug/l 98 80) 1,3,5-Trimethylbenzene 11.51 105 3634 0.37 ug/l 100 84) 1,2,4-Trimethylbenzene 11.81 105 11273 1.13 ug/l 98 85) sec-Butylbenzene 11.95 105 3518 0.30 ug/l 79 88) 1,4-Dichlorobenzene 12.10 146 7709 1.24 ug/l # 73 95) Naphthalene 13.84 128 26655 2.13 ug/l # 92 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed