Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001519.D Acq On : 08 May 2018 17:33 Operator : JC/MD Sample : J2644-12 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 13 Sample Multiplier: 1 Quant Time: May 10 11:21:57 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 231698 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 319047 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 279075 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 152184 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 195507 58.71 ug/l 0.00 Spiked Amount 50.000 Recovery = 117.42% 35) Dibromofluoromethane 5.51 113 153065 53.94 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.88% 50) Toluene-d8 8.72 98 545009 52.61 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.22% 62) 4-Bromofluorobenzene 11.15 95 180299 45.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.68% Target Compounds Qvalue 4) Vinyl Chloride 1.40 62 1364 0.43 ug/l 93 27) cis-1,2-Dichloroethene 4.60 96 72242 23.71 ug/l 87 44) Trichloroethene 7.22 130 26595 7.34 ug/l 97 64) Tetrachloroethene 9.34 164 15774 4.06 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed