Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001533.D Acq On : 09 May 2018 00:41 Operator : JC/MD Sample : J2671-02 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 29 Sample Multiplier: 1 Quant Time: May 09 07:50:03 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 242694 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 324056 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 285110 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 152471 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 161742 46.37 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.74% 35) Dibromofluoromethane 5.51 113 126741 43.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.94% 50) Toluene-d8 8.72 98 449183 42.69 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.38% 62) 4-Bromofluorobenzene 11.14 95 145051 35.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.82% Target Compounds Qvalue 16) Acetone 2.45 43 5978 3.77 ug/l 91 18) Methyl Acetate 2.78 43 5809 1.40 ug/l 93 20) Methylene Chloride 2.86 84 17363 5.54 ug/l 98 44) Trichloroethene 7.22 130 18116 4.92 ug/l 94 68) m/p-Xylenes 10.36 106 10564 1.95 ug/l 97 95) Naphthalene 13.84 128 167024 14.79 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed