Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001534.D Acq On : 09 May 2018 01:08 Operator : JC/MD Sample : J2671-04 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 30 Sample Multiplier: 1 Quant Time: May 09 07:52:10 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 244543 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 335810 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 294541 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 164790 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 166375 47.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.66% 35) Dibromofluoromethane 5.51 113 128274 42.94 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.88% 50) Toluene-d8 8.72 98 457616 41.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.94% 62) 4-Bromofluorobenzene 11.14 95 151008 36.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.16% Target Compounds Qvalue 16) Acetone 2.45 43 6404 4.01 ug/l 98 18) Methyl Acetate 2.78 43 5892 1.41 ug/l 91 20) Methylene Chloride 2.86 84 3348 1.06 ug/l # 90 95) Naphthalene 13.84 128 117472 9.62 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed