Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001535.D Acq On : 09 May 2018 01:35 Operator : JC/MD Sample : J2674-02 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 31 Sample Multiplier: 1 Quant Time: May 09 07:53:49 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 237479 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 326449 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 292623 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 163759 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 163373 47.86 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.72% 35) Dibromofluoromethane 5.51 113 125215 43.12 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.24% 50) Toluene-d8 8.72 98 453481 42.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.58% 62) 4-Bromofluorobenzene 11.14 95 150278 36.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.86% Target Compounds Qvalue 16) Acetone 2.45 43 8814 5.69 ug/l 96 18) Methyl Acetate 2.78 43 5933 1.46 ug/l 96 20) Methylene Chloride 2.86 84 9619503 3134.64 ug/l 96 84) 1,2,4-Trimethylbenzene 11.81 105 26029 2.68 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed