Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001536.D Acq On : 09 May 2018 02:01 Operator : JC/MD Sample : J2676-02 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 32 Sample Multiplier: 1 Quant Time: May 09 07:55:22 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 243684 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 334305 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 295515 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 168073 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 165786 47.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.66% 35) Dibromofluoromethane 5.51 113 129321 43.49 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.98% 50) Toluene-d8 8.72 98 466177 42.95 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.90% 62) 4-Bromofluorobenzene 11.14 95 155546 37.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.66% Target Compounds Qvalue 16) Acetone 2.45 43 3834 2.41 ug/l 98 18) Methyl Acetate 2.78 43 5103 1.22 ug/l 97 20) Methylene Chloride 2.86 84 18692 5.94 ug/l 97 67) Ethyl Benzene 10.26 91 17661 1.24 ug/l 99 68) m/p-Xylenes 10.36 106 5701 1.02 ug/l 98 69) o-Xylene 10.70 106 5705 1.05 ug/l 99 84) 1,2,4-Trimethylbenzene 11.81 105 20182 2.03 ug/l 96 95) Naphthalene 13.84 128 524236 42.11 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed