Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001537.D Acq On : 09 May 2018 02:28 Operator : JC/MD Sample : J2676-04 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 33 Sample Multiplier: 1 Quant Time: May 09 07:57:21 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 238537 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 331248 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 287556 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 156062 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 160479 46.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.62% 35) Dibromofluoromethane 5.51 113 125120 42.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.94% 50) Toluene-d8 8.72 98 453691 42.18 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.36% 62) 4-Bromofluorobenzene 11.14 95 146653 35.52 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.04% Target Compounds Qvalue 16) Acetone 2.45 43 4487 2.88 ug/l 100 18) Methyl Acetate 2.78 43 5317 1.30 ug/l 95 20) Methylene Chloride 2.86 84 2067785 670.83 ug/l 99 95) Naphthalene 13.84 128 116041 10.04 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed