Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001538.D Acq On : 09 May 2018 02:55 Operator : JC/MD Sample : J2676-06 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 34 Sample Multiplier: 1 Quant Time: May 09 07:59:42 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 242285 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 328211 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 293711 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 162743 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 161976 46.51 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.02% 35) Dibromofluoromethane 5.51 113 125843 43.11 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.22% 50) Toluene-d8 8.72 98 456273 42.82 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.64% 62) 4-Bromofluorobenzene 11.14 95 149913 36.65 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.30% Target Compounds Qvalue 16) Acetone 2.45 43 3983 2.52 ug/l # 85 18) Methyl Acetate 2.78 43 4561 1.10 ug/l 91 20) Methylene Chloride 2.86 84 5157 1.65 ug/l 94 95) Naphthalene 13.84 128 65458 5.43 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed