Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001539.D Acq On : 09 May 2018 03:21 Operator : JC/MD Sample : J2676-08 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 35 Sample Multiplier: 1 Quant Time: May 09 08:01:05 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 244565 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 334088 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 296001 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 163290 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 163917 46.63 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.26% 35) Dibromofluoromethane 5.51 113 127091 42.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.54% 50) Toluene-d8 8.72 98 462669 42.65 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.30% 62) 4-Bromofluorobenzene 11.14 95 152268 36.57 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.14% Target Compounds Qvalue 16) Acetone 2.45 43 4433 2.78 ug/l 98 18) Methyl Acetate 2.78 43 4213 1.00 ug/l # 90 20) Methylene Chloride 2.86 84 3469 1.10 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed