Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001540.D Acq On : 09 May 2018 03:48 Operator : JC/MD Sample : J2677-04 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 36 Sample Multiplier: 1 Quant Time: May 09 08:02:14 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 244675 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 335951 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 297751 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 164700 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 166128 47.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.48% 35) Dibromofluoromethane 5.51 113 128560 43.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.04% 50) Toluene-d8 8.72 98 464068 42.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.10% 62) 4-Bromofluorobenzene 11.14 95 153580 36.68 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.36% Target Compounds Qvalue 16) Acetone 2.45 43 5891 3.69 ug/l 99 18) Methyl Acetate 2.78 43 6124 1.46 ug/l 99 20) Methylene Chloride 2.86 84 6742 2.13 ug/l 95 95) Naphthalene 13.84 128 38845 3.18 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed