Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001542.D Acq On : 09 May 2018 04:41 Operator : JC/MD Sample : J2759-06 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 38 Sample Multiplier: 1 Quant Time: May 09 08:05:21 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 249586 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 343250 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 309948 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 175546 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 170633 47.57 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.14% 35) Dibromofluoromethane 5.51 113 132152 43.28 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.56% 50) Toluene-d8 8.72 98 477447 42.84 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.68% 62) 4-Bromofluorobenzene 11.14 95 158733 37.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.20% Target Compounds Qvalue 16) Acetone 2.45 43 5240 3.22 ug/l 95 18) Methyl Acetate 2.78 43 6148 1.44 ug/l 98 20) Methylene Chloride 2.86 84 30873 9.57 ug/l 98 44) Trichloroethene 7.22 130 25635 6.58 ug/l 99 68) m/p-Xylenes 10.36 106 6480 1.10 ug/l 99 95) Naphthalene 13.84 128 16243 1.25 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed