Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001544.D Acq On : 09 May 2018 05:35 Operator : JC/MD Sample : J2780-06 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 40 Sample Multiplier: 1 Quant Time: May 09 08:07:44 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 250051 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 337881 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 305401 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 172815 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 168225 46.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.62% 35) Dibromofluoromethane 5.51 113 131976 43.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.82% 50) Toluene-d8 8.72 98 472761 43.09 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.18% 62) 4-Bromofluorobenzene 11.14 95 156320 37.12 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.24% Target Compounds Qvalue 16) Acetone 2.45 43 5086 3.12 ug/l 95 18) Methyl Acetate 2.79 43 6233 1.45 ug/l 98 20) Methylene Chloride 2.86 84 36126 11.18 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed