Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001545.D Acq On : 09 May 2018 06:01 Operator : JC/MD Sample : J2783-03 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 41 Sample Multiplier: 1 Quant Time: May 09 08:08:36 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 251085 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 342308 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 309285 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 177205 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 169915 47.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.16% 35) Dibromofluoromethane 5.51 113 130181 42.76 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.52% 50) Toluene-d8 8.72 98 475782 42.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.62% 62) 4-Bromofluorobenzene 11.14 95 157476 36.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.82% Target Compounds Qvalue 16) Acetone 2.45 43 10835 6.61 ug/l 96 20) Methylene Chloride 2.86 84 28095 8.66 ug/l 93 95) Naphthalene 13.84 128 33488 2.55 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed