Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001546.D Acq On : 09 May 2018 06:28 Operator : JC/MD Sample : J2783-06 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 42 Sample Multiplier: 1 Quant Time: May 09 08:14:48 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 249859 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 342322 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 308219 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 176709 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 170174 47.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.78% 35) Dibromofluoromethane 5.51 113 131289 43.12 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.24% 50) Toluene-d8 8.72 98 474119 42.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.32% 62) 4-Bromofluorobenzene 11.14 95 158169 37.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.14% Target Compounds Qvalue 16) Acetone 2.45 43 9239 5.67 ug/l 98 18) Methyl Acetate 2.78 43 7100 1.66 ug/l 100 20) Methylene Chloride 2.86 84 74267 23.00 ug/l 98 95) Naphthalene 13.84 128 19486 1.49 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed