Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050818\ Data File : VX001547.D Acq On : 09 May 2018 06:54 Operator : JC/MD Sample : J2784-02 5X Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 43 Sample Multiplier: 1 Quant Time: May 09 08:16:10 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 253936 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 345896 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 313550 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 174401 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 171320 46.94 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.88% 35) Dibromofluoromethane 5.51 113 133438 43.37 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.74% 50) Toluene-d8 8.72 98 486717 43.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 86.68% 62) 4-Bromofluorobenzene 11.14 95 160660 37.27 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.54% Target Compounds Qvalue 16) Acetone 2.45 43 5218 3.15 ug/l 96 18) Methyl Acetate 2.78 43 6797 1.56 ug/l 99 20) Methylene Chloride 2.86 84 44768 13.64 ug/l 97 44) Trichloroethene 7.22 130 4177 1.06 ug/l 87 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed