Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001555.D Acq On : 09 May 2018 14:22 Operator : JC/MD Sample : VX0509WBL01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 4 Sample Multiplier: 1 Quant Time: May 10 04:40:22 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 250433 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 340085 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 298481 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 163276 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 207482 57.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 115.28% 35) Dibromofluoromethane 5.51 113 164486 54.38 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.76% 50) Toluene-d8 8.72 98 594810 53.87 ug/l 0.00 Spiked Amount 50.000 Recovery = 107.74% 62) 4-Bromofluorobenzene 11.14 95 193491 45.65 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.30% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed