Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001556.D Acq On : 09 May 2018 15:46 Operator : JC/MD Sample : J2732-12 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 5 Sample Multiplier: 1 Quant Time: May 10 04:42:35 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 250130 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 342306 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 297938 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 156349 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 204946 57.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 114.02% 35) Dibromofluoromethane 5.51 113 158516 52.06 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.12% 50) Toluene-d8 8.72 98 566696 50.99 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.98% 62) 4-Bromofluorobenzene 11.14 95 183173 42.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 85.86% Target Compounds Qvalue 16) Acetone 2.45 43 12791 7.84 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed