Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001557.D Acq On : 09 May 2018 16:12 Operator : JC/MD Sample : J2732-01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 6 Sample Multiplier: 1 Quant Time: May 10 04:43:57 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 246381 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 337043 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 290312 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 159722 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 204977 57.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 115.76% 35) Dibromofluoromethane 5.51 113 159376 53.16 ug/l 0.00 Spiked Amount 50.000 Recovery = 106.32% 50) Toluene-d8 8.72 98 563002 51.45 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.90% 62) 4-Bromofluorobenzene 11.14 95 184467 43.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 87.82% Target Compounds Qvalue 16) Acetone 2.45 43 9741 6.06 ug/l 97 40) Benzene 6.15 78 4271 0.34 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed