Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\Data\VX050918\ Data File : VX001559.D Acq On : 09 May 2018 17:06 Operator : JC/MD Sample : J2659-01RE Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 8 Sample Multiplier: 1 Quant Time: May 10 04:47:53 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 236274 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 323693 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 278183 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 146138 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 190091 55.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 111.94% 35) Dibromofluoromethane 5.51 113 148727 51.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 103.32% 50) Toluene-d8 8.72 98 529455 50.38 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.76% 62) 4-Bromofluorobenzene 11.14 95 169394 41.99 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.98% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed