Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001561.D Acq On : 09 May 2018 17:59 Operator : JC/MD Sample : J2732-05 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 10 Sample Multiplier: 1 Quant Time: May 10 12:32:12 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 234451 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 319637 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 269214 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 138178 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 193097 57.30 ug/l 0.00 Spiked Amount 50.000 Recovery = 114.60% 35) Dibromofluoromethane 5.51 113 150233 52.84 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.68% 50) Toluene-d8 8.72 98 527741 50.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.70% 62) 4-Bromofluorobenzene 11.14 95 165217 41.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 82.94% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed