Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001568.D Acq On : 09 May 2018 21:07 Operator : JC/MD Sample : J2732-02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 17 Sample Multiplier: 1 Quant Time: May 10 12:36:09 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 226269 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 310260 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 267592 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 134050 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 190336 58.53 ug/l 0.00 Spiked Amount 50.000 Recovery = 117.06% 35) Dibromofluoromethane 5.51 113 150281 54.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 108.92% 50) Toluene-d8 8.72 98 513992 51.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 102.04% 62) 4-Bromofluorobenzene 11.14 95 159746 41.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 82.62% Target Compounds Qvalue 30) Chloroform 5.23 83 115086 22.93 ug/l 99 38) Carbon Tetrachloride 5.79 117 25468 6.05 ug/l 98 46) Dibromomethane 7.67 93 2736 1.34 ug/l 95 47) Bromodichloromethane 7.91 83 23579 6.26 ug/l 99 60) Dibromochloromethane 9.59 129 14131 4.54 ug/l 99 71) Bromoform 10.86 173 7748 6.23 ug/l # 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed