Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001570.D Acq On : 09 May 2018 22:00 Operator : JC/MD Sample : J2732-04 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 19 Sample Multiplier: 1 Quant Time: May 10 12:40:07 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 232755 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 315934 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 276915 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 146790 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 188777 56.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 112.86% 35) Dibromofluoromethane 5.51 113 148036 52.68 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.36% 50) Toluene-d8 8.72 98 518281 50.53 ug/l 0.00 Spiked Amount 50.000 Recovery = 101.06% 62) 4-Bromofluorobenzene 11.14 95 165990 42.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 84.30% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed