Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX050918\ Data File : VX001574.D Acq On : 10 May 2018 00:14 Operator : JC/MD Sample : VX0509MBL01 Misc : 5.0g/10mL/100ul/5mL/MSVOA_X/MEOH ALS Vial : 24 Sample Multiplier: 1 Quant Time: May 10 05:10:10 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X050518W.M Quant Title : SW846 8260 QLast Update : Sun May 06 07:59:25 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 234522 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 314896 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 267003 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 131977 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 185300 54.97 ug/l 0.00 Spiked Amount 50.000 Recovery = 109.94% 35) Dibromofluoromethane 5.51 113 146424 52.28 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.56% 50) Toluene-d8 8.72 98 513690 50.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 100.48% 62) 4-Bromofluorobenzene 11.14 95 153391 39.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.16% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed